n,n'-Dimethylbutanediamide

Base Information

• Chemical Name: n,n'-Dimethylbutanediamide
• CAS No.: 16873-50-0
• Molecular Formula: C6H12 N2 O2
• Molecular Weight: 144.173
• Hs Code.: 2924199090
• NSC Number: 57550
• DSSTox Substance ID: DTXSID10937535
• Nikkaji Number: J441.063G
• Mol file: 16873-50-0.mol

Synonyms:n,n'-dimethylbutanediamide;16873-50-0;N,N/'-Dimethylsuccinamide;N,N'-dimethylsuccinamide;NSC57550;SCHEMBL3660629;Succinamide, N,N'-dimethyl-,;DTXSID10937535;NSC-57550;AKOS006347667;N~1~,N~4~-Dimethylbutanediimidic acid

Chemical Property of n,n'-Dimethylbutanediamide

Chemical Property:

• Boiling Point: 429.2°Cat760mmHg
• Flash Point: 209.9°C
• PSA: 58.20000
• Density: 1.033g/cm³
• LogP: 0.04040
• XLogP3: -1.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 144.089877630
• Heavy Atom Count: 10
• Complexity: 118

Purity/Quality:

98%,99%, ^*data from raw suppliers

N,N'-DIMETHYLSUCCINAMIDE AldrichCPR ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CNC(=O)CCC(=O)NC

Technology Process of n,n'-Dimethylbutanediamide

There total 13 articles about n,n'-Dimethylbutanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

Succinimide (123-56-8,89963-74-6) + methylamine (74-89-5) → N,N'-dimethylsuccinamide (16873-50-0)

Guidance literature:

In water; for 72h; Ambient temperature;

Reference yield:

N-methyl-acetamide (79-16-3) → N,N'-diacetylethylenediamine (871-78-3) + N,N'-dimethylsuccinamide (16873-50-0) + N-acetyl-β-alanine N'-methylamide (33233-69-1)

Guidance literature:

In solid; at -196.1 ℃; Product distribution; Mechanism; Irradiation; also in aqueous solution;

DOI:10.1039/f19878300125

Reference yield:

butanedinitrile (110-61-2) + methylamine (74-89-5) → N,N'-dimethylsuccinamide (16873-50-0)

Guidance literature:

With water;

DOI:10.1021/ja01610a007

upstream raw materials:

2,5-hexanedione

succinoyl dichloride

methylamine

butanedinitrile

Downstream raw materials:

N,N'-dimethyl-1,4-butanediamine

methyl nitrate

succinic acid