Germanium, iodotriethyl-

Base Information

• Chemical Name: Germanium, iodotriethyl-
• CAS No.: 13314-51-7
• Molecular Formula: C6H15GeI
• Molecular Weight: 286.68
• DSSTox Substance ID: DTXSID30157975
• Nikkaji Number: J49.116K
• Wikidata: Q83026131
• Mol file: 13314-51-7.mol

Synonyms:Germanium, iodotriethyl-;Triethylgermanium iodide;Germane, triethyliodo-;BRN 4123587;13314-51-7;Triethyliodogermane;C6H15GeI;C6-H15-Ge-I;SCHEMBL10778538;DTXSID30157975;LS-71219

Chemical Property of Germanium, iodotriethyl-

Chemical Property:

• Vapor Pressure: 0.704mmHg at 25°C
• Boiling Point: 191.8°Cat760mmHg
• Flash Point: 59.4°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 287.94303
• Heavy Atom Count: 8
• Complexity: 51.3

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC[Ge](CC)(CC)I

Technology Process of Germanium, iodotriethyl-

There total 4 articles about Germanium, iodotriethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

benzoyl iodide (618-38-2) + N-triethylgermyl-N,N-bis(trimethylsilyl)amine (1357556-77-4) → N,N-bis(trimethylsilyl)benzamide (38850-27-0) + C13H23NOSi2*C6H15GeI + triethyl(iodo)germane (13314-51-7)

Guidance literature:

at 55 - 65 ℃; for 37h;

DOI:10.1134/S1070428013010259

Reference yield:

triethylchlorogermane (994-28-5) + iodomethylbenzene (620-05-3) → triethyl(iodo)germane (13314-51-7) + benzyl chloride (100-44-7)

Guidance literature:

With N-benzyl pyridinium halide; at 50 ℃; Equilibrium constant; var. n-Et₃GeCl/PhCH₂I ratios;

DOI:10.1016/S0022-328X(00)81789-1

Reference yield:

acetyl iodide (507-02-8) + N-triethylgermyl-N,N-bis(trimethylsilyl)amine (1357556-77-4) → triethyl(iodo)germane (13314-51-7) + N,N-bis(trimethylsilyl)acetamide (10416-58-7)

Guidance literature:

at 80 - 90 ℃; for 5h;

DOI:10.1134/S1070428013010259

upstream raw materials:

triethylchlorogermane

iodomethylbenzene

Bromotriethylgermanium

acetyl iodide

Downstream raw materials:

triethylchlorogermane

iodomethylbenzene

Triethylgerman