3,3',4,4'-Tetrachloroazobenzene

Base Information

Chemical Name:3,3',4,4'-Tetrachloroazobenzene
CAS No.:14047-09-7
Molecular Formula:C12H6 Cl4 N2
Molecular Weight:320.005
Hs Code.:2927000090
UNII:PGG7W94GS9
DSSTox Substance ID:DTXSID6026086,DTXSID80860129
Nikkaji Number:J2.741C
Mol file:14047-09-7.mol

Synonyms:3,4,3',4'-tetrachloroazobenzene;3,4,3',4'-tetrachloroazobenzene, (Z)-isomer;TCAB

Suppliers and Price of 3,3',4,4'-Tetrachloroazobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of 3,3',4,4'-Tetrachloroazobenzene

Chemical Property:

Melting Point:195.5 °C
Refractive Index:1.6000 (estimate)
Boiling Point:441.6 ºC
Flash Point:220.9 ºC
PSA：24.72000
Density:1.48 g/cm³
LogP:6.71560
XLogP3:6.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:319.925559
Heavy Atom Count:18
Complexity:272

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1N=NC2=CC(=C(C=C2)Cl)Cl)Cl)Cl
Uses 3,3'',4,4''-Tetrachloroazobenzene is used in the synthesis of 3,?4-?dichloroaniline. Dyes and metabolites, Environmental Testing.

Technology Process of 3,3',4,4'-Tetrachloroazobenzene

There total 9 articles about 3,3',4,4'-Tetrachloroazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 95-76-1
m,p-dichloroaniline

: 14047-09-7
3,3',4,4'-tetrachloroazobenzene

Guidance literature:: With sodium perborate; sodium molybdate tetrahydrate; In acetic acid; at 50 ℃; for 1h; Temperature; Kinetics; Thermodynamic data; Catalytic behavior;
DOI:10.1007/s11696-018-0599-z

Reference yield: 22.0%

: 95-76-1
m,p-dichloroaniline

: 21232-47-3,125322-31-8
3,3',4,4'-Tetrachloroazoxybenzene

: 3,4,6,7-tetrachlorophenazine

: 1,2,6,7-tetrachlorophenazine

: 14047-09-7
3,3',4,4'-tetrachloroazobenzene

Guidance literature:: With dihydrogen peroxide; iron(III) tetrasulfonatophthalocyanine; In water; acetone; at 20 ℃; for 1h; pH=7; Further Variations:; Reagents; reaction time; Product distribution;
DOI:10.1002/(sici)1099-0682(199912)1999:12<2319::aid-ejic2319>3.0.co;2-1