2-(4-Chloro-3-methylphenoxy)acetohydrazide

Base Information

• Chemical Name: 2-(4-Chloro-3-methylphenoxy)acetohydrazide
• CAS No.: 72293-68-6
• Molecular Formula: C9H11 Cl N2 O2
• Molecular Weight: 214.652
• DSSTox Substance ID: DTXSID20222621
• Wikidata: Q83100919
• Mol file: 72293-68-6.mol

Synonyms:2-(4-chloro-3-methylphenoxy)acetohydrazide;72293-68-6;BRN 4683390;(4-chloro-3-methyl-phenoxy)-acetic acid hydrazide;(4-Chloro-3-methylphenoxy)acetic acid hydrazide;Acetic acid, (4-chloro-3-methylphenoxy)-, hydrazide;MFCD00705189;(4-Chloro-3-methyl-phenoxy)acetic acid hydrazide;CBMicro_019307;Cambridge id 5366578;Oprea1_253760;DTXSID20222621;CCG-7540;BBL015538;STK074983;AKOS000116268;VS-04962;BIM-0019400.P001;UPCMLD0ENAT0507-4555:001;2-(4-chloro-3-methylphenoxy) acetohydrazide;CS-0207115;EN300-03632;AB00083209-01;SR-01000207245;SR-01000207245-1;Z56823445;F3095-0212;4-Isoxazolecarboxylic acid, 5-(fluoromethyl)-3-phenyl-, ethyl ester

Chemical Property of 2-(4-Chloro-3-methylphenoxy)acetohydrazide

Chemical Property:

• Vapor Pressure: 8.43E-08mmHg at 25°C
• Boiling Point: 435.9°C at 760 mmHg
• Flash Point: 217.4°C
• Density: 1.279g/cm³
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 214.0509053
• Heavy Atom Count: 14
• Complexity: 201

Purity/Quality:

98%min ^*data from raw suppliers

2-(4-Chloro-3-methylphenoxy)acetohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1)OCC(=O)NN)Cl

Technology Process of 2-(4-Chloro-3-methylphenoxy)acetohydrazide

There total 3 articles about 2-(4-Chloro-3-methylphenoxy)acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Methyl 4-chloro-3-methylphenoxyacetate (117554-55-9) → 2-(4-chloro-3-methylphenoxy)acetohydrazide (72293-68-6)

Guidance literature:

With hydrazine hydrate; In ethanol; for 5h; Heating;

Reference yield: 85.0%

ethyl 2-(4-chloro-3-methylphenoxy)acetate (30406-61-2) → 2-(4-chloro-3-methylphenoxy)acetohydrazide (72293-68-6)

Guidance literature:

With hydrazine hydrate; In ethanol; for 6h; Reflux;

Reference yield:

4-Chloro-3-methylphenol (59-50-7) → 2-(4-chloro-3-methylphenoxy)acetohydrazide (72293-68-6)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / 16 h / Heating

2: hydrazine hydrate (99percent) / ethanol / 8 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; acetone;

upstream raw materials:

Methyl 4-chloro-3-methylphenoxyacetate

ethyl 2-(4-chloro-3-methylphenoxy)acetate

4-Chloro-3-methylphenol

Downstream raw materials:

2-(3'-methyl-4'-chlorophenoxymethyl)-Δ²-1,3,4-oxadiazoline-5-thione

C₁₈H₂₀ClN₃O₂S

2-Amino-5-(4'-chloro-3'-methylphenoxymethyl)-1,3,4-oxadiazole

(4-Chloro-3-methyl-phenoxy)-acetic acid [2-oxo-1,2-dihydro-indol-(3Z)-ylidene]-hydrazide

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