2-Propenoic acid, 3,3'-thiobis-, diethyl ester, (E,E)-

Base Information

Chemical Name:2-Propenoic acid, 3,3'-thiobis-, diethyl ester, (E,E)-
CAS No.:20626-40-8
Molecular Formula:C10H14 O4 S
Molecular Weight:230.285
Hs Code.:2930909090
European Community (EC) Number:243-926-2
DSSTox Substance ID:DTXSID601239408
Nikkaji Number:J1.523.825I,J342.535E
Mol file:20626-40-8.mol

Synonyms:20626-40-8;EINECS 243-926-2;2-Propenoic acid, 3,3'-thiobis-, diethyl ester, (E,E)-;Diethyl (E,E)-3,3'-thiobisacrylate;2-Propenoic acid, 3,3'-thiobis-, 1,1'-diethyl ester, (2E,2'E)-;DTXSID601239408;Diethyl(E,E)-3,3'-thiobisacrylate;AKOS024379824;3,3'-Thiobis(acrylic acid ethyl) ester;3,3'-Thiodi[(E)-acrylic acid ethyl] ester;1,1'-Diethyl (2E,2'E)-3,3'-thiobis[2-propenoate]

Suppliers and Price of 2-Propenoic acid, 3,3'-thiobis-, diethyl ester, (E,E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Propenoic acid, 3,3'-thiobis-, diethyl ester, (E,E)-

Chemical Property:

Boiling Point:311.4°Cat760mmHg
Flash Point:140.3°C
PSA：77.90000
Density:1.141g/cm³
LogP:1.87320
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:230.06128010
Heavy Atom Count:15
Complexity:232

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C=CSC=CC(=O)OCC
Isomeric SMILES:CCOC(=O)/C=C/S/C=C/C(=O)OCC

Technology Process of 2-Propenoic acid, 3,3'-thiobis-, diethyl ester, (E,E)-

There total 4 articles about 2-Propenoic acid, 3,3'-thiobis-, diethyl ester, (E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 623-47-2
propynoic acid ethyl ester

: 53229-47-3
diethyl thiophene-3,4-dicarboxylate

: 20626-40-8
trans,trans-Thio-β,β'-(acrylsaeure-ethylester)

: 103625-37-2
1,3,5-tricarboethoxy-2,4,6-trimercaptobenzene

Guidance literature:: With sodium perchlorate; In N,N-dimethyl-formamide; Ambient temperature; cathode: S-C, working potencial: -0.9 V, current intensity at the beginning: 200 mA;
DOI:10.1016/S0040-4039(00)84502-5

Reference yield:

: 20626-39-5
(Z,Z)-Bis[2-(ethoxycarbonyl)-1-ethenyl]sulfane

: 20626-40-8
trans,trans-Thio-β,β'-(acrylsaeure-ethylester)

Guidance literature:: at 150 ℃; under 100 Torr;

Reference yield:

: 16490-99-6
ethyl (Z)-3-chloro-2-propenoate

: 20626-40-8
trans,trans-Thio-β,β'-(acrylsaeure-ethylester)

Guidance literature:: Multi-step reaction with 2 steps

1: CS₂, NH₃ / ethanol

2: 150 °C / 100 Torr

With carbon disulfide; ammonia; In ethanol;