1-Azido-2,3,4,6-tetrafluoro-5-iodobenzene

Base Information

Chemical Name:1-Azido-2,3,4,6-tetrafluoro-5-iodobenzene
CAS No.:923294-26-2
Molecular Formula:C6F4IN3
Molecular Weight:316.984
Hs Code.:
DSSTox Substance ID:DTXSID40582931
Nikkaji Number:J2.444.340J
Wikidata:Q82474439

Synonyms:1-Azido-2,3,4,6-tetrafluoro-5-iodobenzene;923294-26-2;DTXSID40582931

Suppliers and Price of 1-Azido-2,3,4,6-tetrafluoro-5-iodobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Azido-2,3,4,6-tetrafluoro-5-iodobenzene

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:1
Exact Mass:316.90731
Heavy Atom Count:14
Complexity:260

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1(=C(C(=C(C(=C1F)I)F)F)F)N=[N+]=[N-]

Technology Process of 1-Azido-2,3,4,6-tetrafluoro-5-iodobenzene

There total 3 articles about 1-Azido-2,3,4,6-tetrafluoro-5-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 923294-22-8
3-iodo-2,4,5,6-tetrafluoroaniline

: 923294-26-2
3-iodo-2,4,5,6-tetrafluoroazidobenzene

Guidance literature:: With trifluoroacetic acid; sodium nitrite; In water; at -5 ℃; for 0.5h;
DOI:10.1021/jo061624b

Reference yield:

: 314-41-0
1,2,3,5-tetrafluoro-4-nitrobenzene

: 923294-26-2
3-iodo-2,4,5,6-tetrafluoroazidobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / H₅IO₆; H₂SO₄; KI / 4 h / 0 - 50 °C

2: 81 percent / hydrogen / palladium on carbon / methanol / 1 h / 3000.24 Torr

3: 84 percent / trifluoroacetic acid; sodium nitrite / H₂O / 0.5 h / -5 °C

With sulfuric acid; hydrogen; periodic acid; trifluoroacetic acid; potassium iodide; sodium nitrite; palladium on activated charcoal; In methanol; water;
DOI:10.1021/jo061624b

Reference yield:

: 71451-49-5
1,2,3,5-tetrafluoro-4-iodo-6-nitrobenzene

: 923294-26-2
3-iodo-2,4,5,6-tetrafluoroazidobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / hydrogen / palladium on carbon / methanol / 1 h / 3000.24 Torr

2: 84 percent / trifluoroacetic acid; sodium nitrite / H₂O / 0.5 h / -5 °C

With hydrogen; trifluoroacetic acid; sodium nitrite; palladium on activated charcoal; In methanol; water;
DOI:10.1021/jo061624b