Technology Process of 2,4,5,6-tetrafluoro-3-iodophenylnitrene
There total 4 articles about 2,4,5,6-tetrafluoro-3-iodophenylnitrene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 92 percent / H5IO6; H2SO4; KI / 4 h / 0 - 50 °C
2: 81 percent / hydrogen / palladium on carbon / methanol / 1 h / 3000.24 Torr
3: 84 percent / trifluoroacetic acid; sodium nitrite / H2O / 0.5 h / -5 °C
4: Photolysis
With
sulfuric acid; hydrogen; periodic acid; trifluoroacetic acid; potassium iodide; sodium nitrite;
palladium on activated charcoal;
In
methanol; water;
DOI:10.1021/jo061624b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 81 percent / hydrogen / palladium on carbon / methanol / 1 h / 3000.24 Torr
2: 84 percent / trifluoroacetic acid; sodium nitrite / H2O / 0.5 h / -5 °C
3: Photolysis
With
hydrogen; trifluoroacetic acid; sodium nitrite;
palladium on activated charcoal;
In
methanol; water;
DOI:10.1021/jo061624b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 84 percent / trifluoroacetic acid; sodium nitrite / H2O / 0.5 h / -5 °C
2: Photolysis
With
trifluoroacetic acid; sodium nitrite;
In
water;
DOI:10.1021/jo061624b
