2,4-Hexadienoic acid, 4-ethyl-, ethyl ester, (2E,4E)-

Base Information

Chemical Name:2,4-Hexadienoic acid, 4-ethyl-, ethyl ester, (2E,4E)-
CAS No.:92454-22-3
Molecular Formula:C₁₀H₁₆O₂
Molecular Weight:168.236
Hs Code.:

Synonyms:

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Chemical Property of 2,4-Hexadienoic acid, 4-ethyl-, ethyl ester, (2E,4E)-

Chemical Property:

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Technology Process of 2,4-Hexadienoic acid, 4-ethyl-, ethyl ester, (2E,4E)-

There total 1 articles about 2,4-Hexadienoic acid, 4-ethyl-, ethyl ester, (2E,4E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17145-91-4
triethyl 2-ethylphosphonoacetate

: 123-11-5
4-methoxy-benzaldehyde

: 92454-22-3
ethyl (E,E)-4-ethylhexa-2,4-dienoate

: 162213-19-6
ethyl 2-((E)-4-methoxybenzylidene)butyrate

Guidance literature:

Reference yield:

: 92454-22-3
ethyl (E,E)-4-ethylhexa-2,4-dienoate

: 1334496-29-5
2-((1S,2R,3S)-4-ethyl-2-nitro-1,2,3,6-tetrahydro-[1,1'-biphenyl]-3-yl)acetaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide

3: (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; o-fluoro-benzoic acid / chloroform / 10 h / 55 °C

With (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; diisobutylaluminium hydride; o-fluoro-benzoic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In chloroform; dimethyl sulfoxide; toluene; 3: Diels-Alder reaction;
DOI:10.1002/anie.201102013

Reference yield:

: 92454-22-3
ethyl (E,E)-4-ethylhexa-2,4-dienoate

: C₁₆H₂₁NO₃

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide

3: (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; o-fluoro-benzoic acid / chloroform / 10 h / 55 °C

4: sodium tetrahydroborate / methanol / 25 °C

With (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; sodium tetrahydroborate; diisobutylaluminium hydride; o-fluoro-benzoic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; chloroform; dimethyl sulfoxide; toluene; 3: Diels-Alder reaction;
DOI:10.1002/anie.201102013