1,5,9-Triazacyclododecane-1,5-dicarboxylic acid, 9-[(2S)-2-carboxy-2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, 1,5-bis(1,1-dimethylethyl) ester

Base Information

Chemical Name:1,5,9-Triazacyclododecane-1,5-dicarboxylic acid, 9-[(2S)-2-carboxy-2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, 1,5-bis(1,1-dimethylethyl) ester
CAS No.:924645-00-1
Molecular Formula:C30H48N4O8
Molecular Weight:592.733
Hs Code.:

1,5,9-Triazacyclododecane-1,5-dicarboxylic acid,
9-[(2S)-2-carboxy-2-[[(phenylmethoxy)carbonyl]amino]ethyl]-,
1,5-bis(1,1-dimethylethyl) ester

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Chemical Property of 1,5,9-Triazacyclododecane-1,5-dicarboxylic acid, 9-[(2S)-2-carboxy-2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, 1,5-bis(1,1-dimethylethyl) ester

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Technology Process of 1,5,9-Triazacyclododecane-1,5-dicarboxylic acid, 9-[(2S)-2-carboxy-2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, 1,5-bis(1,1-dimethylethyl) ester

There total 1 articles about 1,5,9-Triazacyclododecane-1,5-dicarboxylic acid, 9-[(2S)-2-carboxy-2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, 1,5-bis(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 26054-60-4
((S)-2-Oxo-oxetan-3-yl)-carbamic acid benzyl ester

: 174192-40-6
bis(1,1-dimethylethyl) 1,5,9-triazacyclododecane-1,5-dicarboxylate

: 924645-00-1
9-(2-benzyloxycarbonylamino-2-carboxy-ethyl)-1,5,9triaza-cyclododecane-1,5-dicarboxylic acid di-tert-butyl ester

Guidance literature:: In acetonitrile; at 40 ℃; for 168h;
DOI:10.1021/jo061754k

Reference yield: 90.0%

: 924645-00-1
9-(2-benzyloxycarbonylamino-2-carboxy-ethyl)-1,5,9triaza-cyclododecane-1,5-dicarboxylic acid di-tert-butyl ester

: 593-51-1
methylamine hydrochloride

: 924644-83-7
(S)-(benzyloxycarbonylamino)-3-[5,9-di(tert-butyloxycarbonyl)-1,5,9-triazacyclododec-1-yl]-N-methylpropionamide

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 144h; pH=10;
DOI:10.1021/jo061754k