Technology Process of 7-ETHOXYINDOLE
There total 1 articles about 7-ETHOXYINDOLE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; potassium iodide;
In
N,N-dimethyl-formamide;
at 90 ℃;
DOI:10.1248/cpb.53.184
- Guidance literature:
-
Multi-step reaction with 4 steps
1: phosphorus oxychloride / 2 h / 20 °C
2: ammonium acetate; Ac2O; AcOH / AcONa / 2 h / Heating
3: LiAlH4 / tetrahydrofuran; diethyl ether / 5.5 h / Heating
4: methanol / 20 °C
With
ammonium acetate; lithium aluminium tetrahydride; acetic anhydride; acetic acid; trichlorophosphate;
sodium acetate;
In
tetrahydrofuran; methanol; diethyl ether;
1: Vilsmeier reaction;
DOI:10.1248/cpb.53.184
- Guidance literature:
-
Multi-step reaction with 3 steps
1: phosphorus oxychloride / 2 h / 20 °C
2: ammonium acetate; Ac2O; AcOH / AcONa / 2 h / Heating
3: LiAlH4 / tetrahydrofuran; diethyl ether / 5.5 h / Heating
With
ammonium acetate; lithium aluminium tetrahydride; acetic anhydride; acetic acid; trichlorophosphate;
sodium acetate;
In
tetrahydrofuran; diethyl ether;
1: Vilsmeier reaction;
DOI:10.1248/cpb.53.184
