1H-Pyrrole-3-propanoic acid, 5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4-methyl-2-[(phenylmethoxy)carbonyl]-, methyl ester

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Chemical Name:1H-Pyrrole-3-propanoic acid, 5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4-methyl-2-[(phenylmethoxy)carbonyl]-, methyl ester
CAS No.:92735-28-9
Molecular Formula:C30H38N2O6
Molecular Weight:522.642
Hs Code.:

1H-Pyrrole-3-propanoic acid,
5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth
yl]-4-methyl-2-[(phenylmethoxy)carbonyl]-, methyl ester

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Chemical Property of 1H-Pyrrole-3-propanoic acid, 5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4-methyl-2-[(phenylmethoxy)carbonyl]-, methyl ester

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Technology Process of 1H-Pyrrole-3-propanoic acid, 5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4-methyl-2-[(phenylmethoxy)carbonyl]-, methyl ester

There total 3 articles about 1H-Pyrrole-3-propanoic acid, 5-[[5-[(1,1-dimethylethoxy)carbonyl]-4-ethyl-3-methyl-1H-pyrrol-2-yl]meth yl]-4-methyl-2-[(phenylmethoxy)carbonyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 75488-16-3
tert-Butyl-(3-ethyl-4-methyl-pyrrolyl-2)-methanoat

: 51671-81-9
2-benzoyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methyl-5-(acetoxymethyl)pyrrole

: 92735-28-9
benzyl 5'-t-butoxycarbonyl-4'-ethyl-4-(2-methoxycarbonylethyl)-3,3'-dimethylpyrromethane-5-carboxylate

Guidance literature:: With toluene-4-sulfonic acid; In acetic acid; at 45 ℃; for 4h;
DOI:10.1016/S0040-4020(01)91126-3

Reference yield:

: 52459-88-8
2-(tert-Butoxycarbonyl)-3-ethyl-4-methylpyrrole-5-carboxylic acid

: 92735-28-9
benzyl 5'-t-butoxycarbonyl-4'-ethyl-4-(2-methoxycarbonylethyl)-3,3'-dimethylpyrromethane-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂, sodium acetate / 10 percent Pd on charcoal / ethanol / 3 h / 2585.7 Torr

2: 60 percent / p-toluensulfonic acid / CH₂Cl₂ / 4 h / 40 °C

With hydrogen; sodium acetate; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)87636-5

Reference yield:

: 33317-06-5
benzyl 3-<2-(methoxycarbonyl)ethyl>-4,5-methylpyrrole-2-carboxylate

: 92735-28-9
benzyl 5'-t-butoxycarbonyl-4'-ethyl-4-(2-methoxycarbonylethyl)-3,3'-dimethylpyrromethane-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / lead tetra-acetate / acetic acid / Ambient temperature

2: 77 percent / p-toluene sulfonic acid hydrate / acetic acid / 4 h / 45 °C

With lead(IV) acetate; toluene-4-sulfonic acid; In acetic acid;
DOI:10.1016/S0040-4020(01)91126-3