Benzoic acid,2-[1-(2-hydroxyphenyl)ethylidene]hydrazide

Base Information

Chemical Name:Benzoic acid,2-[1-(2-hydroxyphenyl)ethylidene]hydrazide
CAS No.:22233-86-9
Molecular Formula:C15H14 N2 O2
Molecular Weight:254.288
Hs Code.:
Mol file:22233-86-9.mol

Synonyms:Benzoicacid, (a-methylsalicylidene)hydrazide(6CI,8CI); Benzoic acid, [1-(2-hydroxyphenyl)ethylidene]hydrazide (9CI);2-Hydroxyacetophenonebenzoylhydrazone; NSC 148189

Suppliers and Price of Benzoic acid,2-[1-(2-hydroxyphenyl)ethylidene]hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Benzoic acid,2-[1-(2-hydroxyphenyl)ethylidene]hydrazide

Chemical Property:

Boiling Point:386.2°Cat760mmHg
Flash Point:144.2°C
Density:1.219g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid,2-[1-(2-hydroxyphenyl)ethylidene]hydrazide

There total 7 articles about Benzoic acid,2-[1-(2-hydroxyphenyl)ethylidene]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 613-94-5
benzoic acid hydrazide

: 22233-86-9
1-(2-hydroxyphenyl)ethanone benzoylhydrazone

Guidance literature:: With aluminium(III) chloride hexahydrate; In water; at 60 ℃; for 5h; Green chemistry;
DOI:10.1007/s00706-019-02488-2

Reference yield:

: C₁₅H₁₃BN₂O₂

: 22233-86-9
1-(2-hydroxyphenyl)ethanone benzoylhydrazone

Guidance literature:: With dihydrogen peroxide; In N,N-dimethyl-formamide; at 25 ℃; for 0.5h; pH=7.4;
DOI:10.1002/anie.202109835

Reference yield:

: 613-94-5
benzoic acid hydrazide

: 308103-40-4
(2-acetylphenyl)boronic acid

: 22233-86-9
1-(2-hydroxyphenyl)ethanone benzoylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: water / 20 °C

2: dihydrogen peroxide / N,N-dimethyl-formamide / 0.5 h / 25 °C / pH 7.4

With dihydrogen peroxide; In water; N,N-dimethyl-formamide;
DOI:10.1002/anie.202109835