1-(4-Bromobutoxy)-3-chlorobenzene

Base Information

• Chemical Name: 1-(4-Bromobutoxy)-3-chlorobenzene
• CAS No.: 23529-80-8
• Molecular Formula: C10H12 Br Cl O
• Molecular Weight: 263.562
• Hs Code.: 29093038
• DSSTox Substance ID: DTXSID20370570
• Wikidata: Q82157700
• Mol file: 23529-80-8.mol

Synonyms:1-(4-bromobutoxy)-3-chlorobenzene;23529-80-8;3-Chlorophenoxybutylbromide;m-(4-bromobutoxy)chlorobenzene;SCHEMBL1281910;DTXSID20370570;NFQQHXYGFYKMQL-UHFFFAOYSA-N

Chemical Property of 1-(4-Bromobutoxy)-3-chlorobenzene

Chemical Property:

• Vapor Pressure: 0.000524mmHg at 25°C
• Refractive Index: 1.552-1.554
• Boiling Point: 322.5°Cat760mmHg
• Flash Point: 148.9°C
• PSA: 9.23000
• Density: 1.401g/cm³
• LogP: 3.89390
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 261.97601
• Heavy Atom Count: 13
• Complexity: 132

Purity/Quality:

98.5% ^*data from raw suppliers

1-(4-BROMOBUTOXY)-3-CHLOROBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 36/37/38-20/22
• Safety Statements: 37/39-26

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)Cl)OCCCCBr

Technology Process of 1-(4-Bromobutoxy)-3-chlorobenzene

There total 2 articles about 1-(4-Bromobutoxy)-3-chlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1,4-dibromo-butane (110-52-1) + 3-monochlorophenol (108-43-0) → 1-(4-bromobutoxy)-3-chlorobenzene (23529-80-8)

Guidance literature:

With sodium hydroxide; In water; at 80 ℃; for 4h;

Reference yield: 40.0%

→ 1-(4-bromobutoxy)-3-chlorobenzene (23529-80-8)

Guidance literature:

Reference yield: 83.0%

1-(4-bromobutoxy)-3-chlorobenzene (23529-80-8) + dimethyl amine (124-40-3) → m-(4-N,N-dimethylaminobutoxy)chlorobenzene

Guidance literature:

With sodium hydroxide; tetrabutylammomium bromide; In water; at 10 - 20 ℃; for 22h;

upstream raw materials:

1,4-dibromo-butane

3-monochlorophenol

Refernces

• 1、 Wang, Lulu,Yang, Wenge,Wang, Kai,Zhu, Jing,Shen, Fei,Hu, Yonghong. "Synthesis and biological evaluation of vinyl ether-containing azole derivatives as inhibitors of Trichophyton rubrum". scheme or table. p. 4887 - 4890. Retrieved 2012/08/07.
• 2、 -. "Aminoalkoxystyrene, process for preparation thereof, polymer thereof, process for producing the polymer and use thereof". Page/Page column 15-16. . Retrieved 2008/06/13.