2-Phenyl-2,3-dihydro-4(1H)-quinazolinethione

Base Information

Chemical Name:2-Phenyl-2,3-dihydro-4(1H)-quinazolinethione
CAS No.:53619-34-4
Molecular Formula:C14H12N2S
Molecular Weight:240.329
Hs Code.:
NSC Number:155614
Nikkaji Number:J3.368.887C

Synonyms:2-Phenyl-2,3-dihydro-4(1H)-quinazolinethione;NSC155614;NSC 155614;53619-34-4;2-phenyl-2,3-dihydro-1H-quinazoline-4-thione;NSC-155614;2-Phenyl-1,2,3,4-tetrahydroquinazoline-4-thione

Suppliers and Price of 2-Phenyl-2,3-dihydro-4(1H)-quinazolinethione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Phenyl-2,3-dihydro-4(1H)-quinazolinethione

Chemical Property:

Vapor Pressure:3.52E-07mmHg at 25°C
Boiling Point:417.5°Cat760mmHg
Flash Point:206.3°C
Density:1.29g/cm³
XLogP3:3.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:240.07211956
Heavy Atom Count:17
Complexity:286

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2NC3=CC=CC=C3C(=S)N2

Technology Process of 2-Phenyl-2,3-dihydro-4(1H)-quinazolinethione

There total 3 articles about 2-Phenyl-2,3-dihydro-4(1H)-quinazolinethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 100-52-7
benzaldehyde

: 2454-39-9
2-aminobenzothioamide

: 53619-34-4
2-phenyl-2,3-dihydroquinazolin-4(1H)-thione

Guidance literature:: In water; at 100 ℃; for 24h; Sealed tube;
DOI:10.1039/c4ob02207f

Reference yield:

: 1885-29-6
anthranilic acid nitrile

: 53619-34-4
2-phenyl-2,3-dihydroquinazolin-4(1H)-thione

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium chloride; sodium hydrogen sulfide monohydrate / N,N-dimethyl-formamide / 72 h / 20 °C / Sealed tube

2: water / 24 h / 100 °C / Sealed tube

With sodium hydrogen sulfide monohydrate; magnesium chloride; In water; N,N-dimethyl-formamide;
DOI:10.1039/c4ob02207f