8-Azabicyclo[3.2.1]octane-3-carboxaldehyde, 8-methyl-, exo- (9CI)

Base Information

Chemical Name:8-Azabicyclo[3.2.1]octane-3-carboxaldehyde, 8-methyl-, exo- (9CI)
CAS No.:93047-52-0
Molecular Formula:C₉H₁₅NO
Molecular Weight:153.224
Hs Code.:
Mol file:93047-52-0.mol

Synonyms:3β-Tropanecarboxaldehyde;8-Azabicyclo[3.2.1]octane-3-carboxaldehyde, 8-methyl-, exo-;

Suppliers and Price of 8-Azabicyclo[3.2.1]octane-3-carboxaldehyde, 8-methyl-, exo- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 8-Azabicyclo[3.2.1]octane-3-carboxaldehyde, 8-methyl-, exo- (9CI)

Chemical Property:

Boiling Point:106-106 °C (11mmHg)
PSA：20.31000
Density:1.089±0.06 g/cm3 (20 °C, 760 mmHg)
LogP:0.99600

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 8-Azabicyclo[3.2.1]octane-3-carboxaldehyde, 8-methyl-, exo- (9CI)

There total 5 articles about 8-Azabicyclo[3.2.1]octane-3-carboxaldehyde, 8-methyl-, exo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 201230-82-2
carbon monoxide

: 529-18-0
tropidine

: 93047-52-0,99658-61-4
Tropan-3β-carboxaldehyd

: 99658-60-3,99658-59-0
8-Methyl-8-aza-bicyclo[3.2.1]octane-2-carbaldehyde

Guidance literature:: With hydrogen; di-μ-chlorobis(norbornadiene)dirhodium(I); triethylamine; triphenylphosphine; In benzene; at 100 ℃; for 6h; under 60004.8 Torr;
DOI:10.1016/0022-328X(86)80440-5

Reference yield: 11.0%

: 201230-82-2
carbon monoxide

: 529-18-0
tropidine

: 529-17-9,687966-22-9
tropane

: 93047-52-0,99658-61-4
Tropan-3β-carboxaldehyd

: 99658-60-3,99658-59-0
8-Methyl-8-aza-bicyclo[3.2.1]octane-2-carbaldehyde

Guidance literature:: With hydrogen; di-μ-chlorobis(norbornadiene)dirhodium(I); tricyclohexylphosphine; In benzene; at 100 ℃; for 6h; under 60004.8 Torr;
DOI:10.1016/0022-328X(86)80440-5

Reference yield: 10.0%

: 201230-82-2
carbon monoxide

: 529-18-0
tropidine

: 529-17-9,687966-22-9
tropane

: 68969-37-9
tropan-2-yl-methanol

: 90949-82-9,888716-28-7
3-hydroxymethyl-8-methyl-8-azabicyclo[3.2.1]octane

: 93047-52-0,99658-61-4
Tropan-3β-carboxaldehyd

: 99658-60-3,99658-59-0
8-Methyl-8-aza-bicyclo[3.2.1]octane-2-carbaldehyde

Guidance literature:: With hydrogen; carbonylhydridetris(triphenylphosphine)rhodium(I); In benzene; at 100 ℃; for 6h; under 60004.8 Torr; Product distribution; various catalysts, formed in situ from various phosphines;
DOI:10.1016/0022-328X(86)80440-5