4-(2-Chloro-3-phenylpropyl)-1,2-dimethoxybenzene

Base Information

Chemical Name:4-(2-Chloro-3-phenylpropyl)-1,2-dimethoxybenzene
CAS No.:93081-21-1
Molecular Formula:C17H19ClO2
Molecular Weight:290.79
Hs Code.:
DSSTox Substance ID:DTXSID30551272

Synonyms:93081-21-1;4-(2-Chloro-3-phenylpropyl)-1,2-dimethoxybenzene;DTXSID30551272

Suppliers and Price of 4-(2-Chloro-3-phenylpropyl)-1,2-dimethoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-Chloro-3-phenylpropyl)-1,2-dimethoxybenzene

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:290.1073575
Heavy Atom Count:20
Complexity:266

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)CC(CC2=CC=CC=C2)Cl)OC

Technology Process of 4-(2-Chloro-3-phenylpropyl)-1,2-dimethoxybenzene

There total 5 articles about 4-(2-Chloro-3-phenylpropyl)-1,2-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 93081-20-0
1-(3,4-dimethoxyphenyl)-3-phenylpropan-2-ol

: 93081-21-1
1-(3,4-dimethoxyphenyl)-3-phenyl-2-propyl chloride

Guidance literature:: With thionyl chloride; In benzene; for 1.5h; Heating;
DOI:10.1135/cccc19841002

Reference yield:

: 93-17-4
3,4-dimethoxyphenylacetonitrile

: 93081-21-1
1-(3,4-dimethoxyphenyl)-3-phenyl-2-propyl chloride

Guidance literature:: Multi-step reaction with 5 steps

1: NaOEt / ethanol / 1)reflux 3.5h 2)stand overnight

2: HCl / acetic acid; H₂O / 1)35 - 50 deg C 2)room temp., 48h

3: 80 percent / 10percentHCl / 6 h / Heating

4: 100 percent / NaBH₄ / ethanol / 5 h / Heating

5: 89 percent / SOCl₂ / benzene / 1.5 h / Heating

With hydrogenchloride; sodium tetrahydroborate; thionyl chloride; sodium ethanolate; In ethanol; water; acetic acid; benzene;
DOI:10.1135/cccc19841002

Reference yield:

: 57543-02-9
1-(3,4-dimethoxyphenyl)-3-phenyl-propan-2-one

: 93081-21-1
1-(3,4-dimethoxyphenyl)-3-phenyl-2-propyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaBH₄ / ethanol / 5 h / Heating

2: 89 percent / SOCl₂ / benzene / 1.5 h / Heating

With sodium tetrahydroborate; thionyl chloride; In ethanol; benzene;
DOI:10.1135/cccc19841002