mu3-Ethylidyne-tris(mu2-hydro)triiron nonacarbonyl

Base Information

Chemical Name:mu3-Ethylidyne-tris(mu2-hydro)triiron nonacarbonyl
CAS No.:69440-00-2
Molecular Formula:C₁₁H₆Fe₃O₉
Molecular Weight:449.704
Hs Code.:

Synonyms:

Suppliers and Price of mu3-Ethylidyne-tris(mu2-hydro)triiron nonacarbonyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of mu3-Ethylidyne-tris(mu2-hydro)triiron nonacarbonyl

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of mu3-Ethylidyne-tris(mu2-hydro)triiron nonacarbonyl

There total 1 articles about mu3-Ethylidyne-tris(mu2-hydro)triiron nonacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112220-73-2
Fe3(μ3-methylidenemethylether)2(carbonyl)9

: 22560-16-3
lithium triethylborohydride

: 17685-52-8
triiron dodecarbonyl

: 103751-58-2
Fe3(μ3-vinylidene)(carbonyl)10

: 112220-75-4
Fe4(μ3-CHCH3)(μ2-carbonyl)(carbonyl)9

: 88610-52-0
HFe(μ3-CCH3)(μ3-carbonyl)(carbonyl)9

: 69440-00-2
(μ-H)3Fe3(μ3-CCH3)(carbonyl)9

Guidance literature:: With CF₃COOH; In tetrahydrofuran; Cooled soln. of Fe complex (-20°C, Ar) is dropwise treated with LiHBEt3 over 5 min, stirring (0.5 h, 1 h without cooling bath), evapn., cooling to -78°C, addn. of CH2Cl2, addn. of CF3COOH, stirring for 15 min, then 15 min at room temp.; Evapn., addn. of n-hexane and H2O, extn. of aq. layer with n-hexane, drying of organic soln. (Na2SO4), chromy. (silica gel, n-hexane, CH2Cl2);