N,N-Diethyl-1-(4-fluorophenyl)-1,1-dimethylstannanamine

Base Information

Chemical Name:N,N-Diethyl-1-(4-fluorophenyl)-1,1-dimethylstannanamine
CAS No.:93247-02-0
Molecular Formula:C12H20FNSn
Molecular Weight:316.006
Hs Code.:
DSSTox Substance ID:DTXSID90532906
Wikidata:Q82405860

Synonyms:93247-02-0;DTXSID90532906;N,N-Diethyl-1-(4-fluorophenyl)-1,1-dimethylstannanamine

Suppliers and Price of N,N-Diethyl-1-(4-fluorophenyl)-1,1-dimethylstannanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N,N-Diethyl-1-(4-fluorophenyl)-1,1-dimethylstannanamine

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:317.060180
Heavy Atom Count:15
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)[Sn](C)(C)C1=CC=C(C=C1)F

Technology Process of N,N-Diethyl-1-(4-fluorophenyl)-1,1-dimethylstannanamine

There total 2 articles about N,N-Diethyl-1-(4-fluorophenyl)-1,1-dimethylstannanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51693-78-8
(CH₃)2Sn(C₆H₄-p-F)I

: 816-43-3
lithium diethylamide

: 93247-02-0
(diethylamino)(p-fluorophenyl)dimethylstannane

Guidance literature:: In pentane; byproducts: LiI; (Ar); dropwise addn. of Sn-compd. in pentane to suspn. of org. compd. in pentane (-15-(-)10°C), heating (10 min), standing (overnight), pptn.; decantation (under Ar), degassing (vac.), washing ppt. with pentane, combining with soln., pentane removal, distn. (vac.); elem. anal.;

Reference yield:

: 693-03-8
n-butyl magnesium bromide

: 51693-78-8
(CH₃)2Sn(C₆H₄-p-F)I

: 109-89-7
diethylamine

: 93247-02-0
(diethylamino)(p-fluorophenyl)dimethylstannane

Guidance literature:: In diethyl ether; pentane; byproducts: butane, MgBrI; (inert atmosphere); slow dropwise addn. of excess of Et2NH to soln. of BuMgBr in ether (-10°C), pptn., warming to room temp., refluxing (20 min), cooling to -15°C, dropwise addn. of Sn-compd. in pentane, heating (1 h), standing (overnight); decanting (under Ar), solvent evapn., distn. (vac.); elem. anal.;