1-methyl-4-{2-[(4-methylphenyl)sulfanyl]benzoyl}piperazine

Base Information

Chemical Name:1-methyl-4-{2-[(4-methylphenyl)sulfanyl]benzoyl}piperazine
CAS No.:93288-91-6
Molecular Formula:C₁₉H₂₂N₂OS
Molecular Weight:326.462
Hs Code.:
Mol file:93288-91-6.mol

Synonyms:(4-Methyl-piperazin-1-yl)-(2-p-tolylsulfanyl-phenyl)-methanone;

Suppliers and Price of 1-methyl-4-{2-[(4-methylphenyl)sulfanyl]benzoyl}piperazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-methyl-4-{2-[(4-methylphenyl)sulfanyl]benzoyl}piperazine

Chemical Property:

Melting Point:87 - 89 °C (light petroleum)
PSA：48.85000
LogP:3.40960

Purity/Quality:

Safty Information:

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Technology Process of 1-methyl-4-{2-[(4-methylphenyl)sulfanyl]benzoyl}piperazine

There total 4 articles about 1-methyl-4-{2-[(4-methylphenyl)sulfanyl]benzoyl}piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-01-3
1-methyl-piperazine

: 93288-91-6
1-methyl-4-<2-(4-methylphenylthio)benzoyl>piperazine

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / CHCl₃ / 1)stirred 1h,room temp. 2)reflux 1h

2: aqueous NH₃

3: Cu,CuI,K₂CO₃ / dimethylformamide / 8 h / Heating

With ammonium hydroxide; copper(l) iodide; copper; potassium carbonate; In chloroform; N,N-dimethyl-formamide;

Reference yield:

: 609-67-6
2-Iodobenzoyl chloride

: 93288-91-6
1-methyl-4-<2-(4-methylphenylthio)benzoyl>piperazine

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / CHCl₃ / 1)stirred 1h,room temp. 2)reflux 1h

2: aqueous NH₃

3: Cu,CuI,K₂CO₃ / dimethylformamide / 8 h / Heating

With ammonium hydroxide; copper(l) iodide; copper; potassium carbonate; In chloroform; N,N-dimethyl-formamide;

Reference yield:

: 93288-84-7
1-(2-iodobenzoyl)-4-methylpiperazine hydrochloride

: 93288-91-6
1-methyl-4-<2-(4-methylphenylthio)benzoyl>piperazine

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous NH₃

2: Cu,CuI,K₂CO₃ / dimethylformamide / 8 h / Heating

With ammonium hydroxide; copper(l) iodide; copper; potassium carbonate; In N,N-dimethyl-formamide;