Technology Process of Benzoic acid, 2-bromo-4,5-dichloro-
There total 5 articles about Benzoic acid, 2-bromo-4,5-dichloro- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuric acid;
In
water; acetic acid;
for 16h;
Heating;
DOI:10.1135/cccc19840992
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99percentHNO3+H2SO4 / 3 h / 40 - 45 °C
2: 67 percent / NH4Cl,Fe / ethanol; H2O / 20 h / Heating
3: NaNO2, H2SO4, CuCl, KCN, Na2CO3 / 1)H2SO4,NaNO2,CH3COOH 10 deg C, 30 min 2) KCN,Na2CO3 in water 2h,20 deg C 3)3h,85 deg C
4: 61 percent / H2SO4 / acetic acid; H2O / 16 h / Heating
With
potassium cyanide; sulfuric acid; nitric acid; iron; sodium carbonate; ammonium chloride; copper(l) chloride; sodium nitrite;
In
ethanol; water; acetic acid;
DOI:10.1135/cccc19840992
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaNO2, H2SO4, CuCl, KCN, Na2CO3 / 1)H2SO4,NaNO2,CH3COOH 10 deg C, 30 min 2) KCN,Na2CO3 in water 2h,20 deg C 3)3h,85 deg C
2: 61 percent / H2SO4 / acetic acid; H2O / 16 h / Heating
With
potassium cyanide; sulfuric acid; sodium carbonate; copper(l) chloride; sodium nitrite;
In
water; acetic acid;
DOI:10.1135/cccc19840992