6-methyl-8-nitrophenanthridine

Base Information

Chemical Name:6-methyl-8-nitrophenanthridine
CAS No.:51381-78-3
Molecular Formula:C14H10N2O2
Molecular Weight:238.2414
Hs Code.:

Synonyms:

Suppliers and Price of 6-methyl-8-nitrophenanthridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 6-methyl-8-nitrophenanthridine

Chemical Property:

Vapor Pressure:2.13E-07mmHg at 25°C
Boiling Point:436°C at 760 mmHg
Flash Point:217.5°C
Density:1.33g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-methyl-8-nitrophenanthridine

There total 9 articles about 6-methyl-8-nitrophenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: (E) methyl o-(p-nitrophenyl)phenyl ketoxime

: 51381-78-3
6-methyl-8-nitrophenanthridine

Guidance literature:: With trifluoromethylsulfonic anhydride; In chlorobenzene; at 0 - 120 ℃; for 17h; Inert atmosphere;
DOI:10.1016/j.tet.2021.132244

Reference yield:

: 2142-69-0
2-bromophenyl methyl ketone

: 51381-78-3
6-methyl-8-nitrophenanthridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

1.2: 18 h / 70 °C

2.1: potassium carbonate; hydroxylamine hydrochloride / ethanol / 18 h / 80 °C

3.1: trifluoromethylsulfonic anhydride / chlorobenzene / 17 h / 0 - 120 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; trifluoromethylsulfonic anhydride; hydroxylamine hydrochloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1016/j.tet.2021.132244

Reference yield:

: 24067-17-2
4-nitrophenylboronic acid

: 51381-78-3
6-methyl-8-nitrophenanthridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

1.2: 18 h / 70 °C

2.1: potassium carbonate; hydroxylamine hydrochloride / ethanol / 18 h / 80 °C

3.1: trifluoromethylsulfonic anhydride / chlorobenzene / 17 h / 0 - 120 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; trifluoromethylsulfonic anhydride; hydroxylamine hydrochloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1016/j.tet.2021.132244