p-Menthane-1,8-diol, diacetate

Base Information

• Chemical Name: p-Menthane-1,8-diol, diacetate
• CAS No.: 20009-20-5
• Molecular Formula: C14H24O4
• Molecular Weight: 256.342
• Hs Code.: 2916209090
• European Community (EC) Number: 243-464-1
• DSSTox Substance ID: DTXSID70864914
• Nikkaji Number: J280.422K
• Mol file: 20009-20-5.mol

Synonyms:p-Menthane-1,8-diol, diacetate;20009-20-5;[4-(2-acetyloxypropan-2-yl)-1-methylcyclohexyl] acetate;4-(Acetoxy)-alpha,alpha,4-trimethylcyclohexylmethyl acetate;AI3-01769;EINECS 243-464-1;AI 3-01769;Cyclohexanemethanol, 4-(acetyloxy)-alpha,alpha,4-trimethyl-, acetate;Cyclohexanemethanol, 4-(acetyloxy)-.alpha.,.alpha.,4-trimethyl-, acetate;Cyclohexanemethanol, 4-(acetyloxy)-alpha,alpha,4-trimethyl-, 1-acetate;Terpin diacetate, trans-;SCHEMBL20296824;DTXSID70864914;Cyclohexanemethanol, 4-(acetyloxy)-?,?,4-trimethyl-, acetate;AKOS040750246;1-[4-(Acetyloxy)-4-methylcyclohexyl]-1-methylethyl acetate #;Cyclohexanemethanol, 4-(acetyloxy)-a,a,4-trimethyl-, acetate;4-(Acetyloxy)-alpha,alpha,4-trimethylcyclohexanemethanol acetate;Cyclohexanemethanol, 4-(acetyloxy)-.alpha.,.alpha.,4-trimethyl-, 1-acetate

Chemical Property of p-Menthane-1,8-diol, diacetate

Chemical Property:

• Boiling Point: 297.8°Cat760mmHg
• Flash Point: 134.9°C
• PSA: 52.60000
• Density: 1.03g/cm³
• LogP: 2.84010
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 256.16745924
• Heavy Atom Count: 18
• Complexity: 325

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OC1(CCC(CC1)C(C)(C)OC(=O)C)C

Technology Process of p-Menthane-1,8-diol, diacetate

There total 3 articles about p-Menthane-1,8-diol, diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-1,8-terpine (565-48-0,89923-77-3) + ethylmagnesium chloride (2386-64-3) → 1,8-diacetoxy-p-menthane (20009-20-5)

Guidance literature:

With diethyl ether; at 0 ℃; diacetate of cis-terpin; Einw_. von Essigsaeureanhydrid auf die Magnesiumverbindung, man zersetzt das Reaktionsprodukt mit Eis;

Reference yield:

1,8-Cineol (65370-78-7) + acetic anhydride (108-24-7) → 1,8-diacetoxy-p-menthane (20009-20-5)

Guidance literature:

With sulfuric acid;

Reference yield:

cis-1,8-terpine (565-48-0,89923-77-3) + sodium acetate (127-09-3) + acetic anhydride (108-24-7) → 1,8-diacetoxy-p-menthane (20009-20-5)

Guidance literature:

upstream raw materials:

cis-1,8-terpine

ethylmagnesium chloride

1,8-Cineol

acetic anhydride