benzyl [(5S,8S,9R,10S,11S,14S)-8,11-dibenzyl-9,10-dihydroxy-15-methyl-3,6,13-trioxo-1-phenyl-5-(propan-2-yl)-2-oxa-4,7,12-triazahexadecan-14-yl]carbamate (non-preferred name)

Base Information

• Chemical Name: benzyl [(5S,8S,9R,10S,11S,14S)-8,11-dibenzyl-9,10-dihydroxy-15-methyl-3,6,13-trioxo-1-phenyl-5-(propan-2-yl)-2-oxa-4,7,12-triazahexadecan-14-yl]carbamate (non-preferred name)
• CAS No.: 129467-50-1
• Molecular Formula: C₄₄H₅₄N₄O₈
• Molecular Weight: 766.935

Synonyms:

Chemical Property of benzyl [(5S,8S,9R,10S,11S,14S)-8,11-dibenzyl-9,10-dihydroxy-15-methyl-3,6,13-trioxo-1-phenyl-5-(propan-2-yl)-2-oxa-4,7,12-triazahexadecan-14-yl]carbamate (non-preferred name)

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 995.9°Cat760mmHg
• Flash Point: 556.1°C
• Density: 1.205g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzyl [(5S,8S,9R,10S,11S,14S)-8,11-dibenzyl-9,10-dihydroxy-15-methyl-3,6,13-trioxo-1-phenyl-5-(propan-2-yl)-2-oxa-4,7,12-triazahexadecan-14-yl]carbamate (non-preferred name)

There total 2 articles about benzyl [(5S,8S,9R,10S,11S,14S)-8,11-dibenzyl-9,10-dihydroxy-15-methyl-3,6,13-trioxo-1-phenyl-5-(propan-2-yl)-2-oxa-4,7,12-triazahexadecan-14-yl]carbamate (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

→ (2S,3R,4S,5S)-2,5-Di-(N-(Cbz-valinyl)amino)-3,4-dihydroxy1,6-diphenylhexane (129467-48-7,129467-49-8,129467-50-1,140385-91-7,142861-15-2)

Guidance literature:

Reference yield:

Z-Val-ONp (10512-93-3) + (2S,3R,4S,5S)-2,5-diamino-3,4-dihydroxy-1,6-diphenylhexane (134878-07-2) → (2S,3R,4S,5S)-2,5-Di-(N-(Cbz-valinyl)amino)-3,4-dihydroxy1,6-diphenylhexane (129467-48-7,129467-49-8,129467-50-1,140385-91-7,142861-15-2)

Guidance literature:

In tetrahydrofuran; for 24h;

DOI:10.1021/jm00055a003

Reference yield:

(2S,3R,4S,5S)-2,5-Di-(N-(Cbz-valinyl)amino)-3,4-dihydroxy1,6-diphenylhexane (129467-48-7,129467-49-8,129467-50-1,140385-91-7,142861-15-2) → (S)-2-Amino-N-[(1S,3R,4S)-4-((S)-2-amino-3-methyl-butyrylamino)-1-benzyl-2,3-dihydroxy-5-phenyl-pentyl]-3-methyl-butyramide

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 4h;

DOI:10.1021/jm00055a003

upstream raw materials:

Z-Val-ONp

(2S,3R,4S,5S)-2,5-diamino-3,4-dihydroxy-1,6-diphenylhexane

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