Benzeneacetic acid, a-[[[1,1-dimethyl-2-[[(4-methylphenyl)sulfonyl]amino]ethyl]methylamino] methylene]-2-(methoxycarbonyl)-, methyl ester, (E)-

Base Information

Chemical Name:Benzeneacetic acid, a-[[[1,1-dimethyl-2-[[(4-methylphenyl)sulfonyl]amino]ethyl]methylamino] methylene]-2-(methoxycarbonyl)-, methyl ester, (E)-
CAS No.:93630-94-5
Molecular Formula:C₂₄H₃₀N₂O₆S
Molecular Weight:474.578
Hs Code.:

Benzeneacetic acid,
a-[[[1,1-dimethyl-2-[[(4-methylphenyl)sulfonyl]amino]ethyl]methylamino]
methylene]-2-(methoxycarbonyl)-, methyl ester, (E)-

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Chemical Property of Benzeneacetic acid, a-[[[1,1-dimethyl-2-[[(4-methylphenyl)sulfonyl]amino]ethyl]methylamino] methylene]-2-(methoxycarbonyl)-, methyl ester, (E)-

Chemical Property:

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Technology Process of Benzeneacetic acid, a-[[[1,1-dimethyl-2-[[(4-methylphenyl)sulfonyl]amino]ethyl]methylamino] methylene]-2-(methoxycarbonyl)-, methyl ester, (E)-

There total 2 articles about Benzeneacetic acid, a-[[[1,1-dimethyl-2-[[(4-methylphenyl)sulfonyl]amino]ethyl]methylamino] methylene]-2-(methoxycarbonyl)-, methyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 716-43-8
dimethyl homophthalate

: 71254-91-6
1-tosyl-3,4,4-trimethyl-Δ²-imidazolinium iodide

: 93630-94-5
2-methoxycarbonyl-α-(methoxycarbonyl)-β-<2-(tosylamino-1,1-dimethyl)ethyl>methylaminostyrene

: 93630-90-1,93630-91-2
2-{Methoxycarbonyl-[3,4,4-trimethyl-1-(toluene-4-sulfonyl)-imidazolidin-2-yl]-methyl}-benzoic acid methyl ester

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -30 ℃; for 0.5h;

Reference yield:

: 131-11-3,64441-70-9
phthalic acid dimethyl ester

: 71254-91-6
1-tosyl-3,4,4-trimethyl-Δ²-imidazolinium iodide

: 93630-94-5
2-methoxycarbonyl-α-(methoxycarbonyl)-β-<2-(tosylamino-1,1-dimethyl)ethyl>methylaminostyrene

: 2-{(R)-Methoxycarbonyl-[(S)-3,4,4-trimethyl-1-(toluene-4-sulfonyl)-imidazolidin-2-yl]-methyl}-benzoic acid methyl ester

: 93630-90-1,93630-91-2
methyl 2(methoxycarbonyl)-α-<2-(1-tosyl-3,4,4-trimethyl)imidazolidinyl>-1-phenylacetate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1) THF, -78 deg C, 20 min, 2) THF, -40 to 0 deg C, 3 h;
DOI:10.1016/S0040-4020(01)96687-6