tert-butyl undec-10-enoate

Base Information

• Chemical Name: tert-butyl undec-10-enoate
• CAS No.: 93757-41-6
• Molecular Formula: C15H28O2
• Molecular Weight: 240.386
• Hs Code.: 2916190090
• Mol file: 93757-41-6.mol

Synonyms:10-Undecenoic acid,1,1-dimethylethyl ester;t-butyl undecenoate;tert-Butyl 10-undecenoate;Undec-10-enoic acid,t-butyl ester;

Chemical Property of tert-butyl undec-10-enoate

Chemical Property:

• PSA: 26.30000
• LogP: 4.63490

Purity/Quality:

99% ^*data from raw suppliers

tert-Butylundec-10-enoate 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl undec-10-enoate

There total 4 articles about tert-butyl undec-10-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

undec-10-enoyl chloride (38460-95-6) + tert-butyl alcohol (75-65-0) → tert-butyl undec-10-enoate (93757-41-6)

Guidance literature:

With triethylamine; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2007.11.071

Reference yield: 86.0%

10-undecenoic acid (112-38-9) + tert-butyl alcohol (75-65-0) → tert-butyl undec-10-enoate (93757-41-6)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1002/anie.201201704

Reference yield: 80.0%

Methyl 10-undecenoate (111-81-9) + tert-butyl alcohol (75-65-0) → tert-butyl undec-10-enoate (93757-41-6)

Guidance literature:

With K5; In toluene; at 85 ℃; for 8h;

DOI:10.1055/s-2006-942456

upstream raw materials:

10-undecenoic acid

tert-butyl alcohol

Methyl 10-undecenoate

undec-10-enoyl chloride

Downstream raw materials:

10-undecenoic acid

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