1-(Isopentyloxy)-3-(2-propynyloxy)-2-propanol carbamate

Base Information

• Chemical Name: 1-(Isopentyloxy)-3-(2-propynyloxy)-2-propanol carbamate
• CAS No.: 14669-16-0
• Molecular Formula: C₁₂H₂₁NO₄
• Molecular Weight: 243.303
• Hs Code.: 2924199090
• Mol file: 14669-16-0.mol

Synonyms:2-Propanol,1-(3-methylbutoxy)-3-(2-propynyloxy)-, carbamate (9CI); 2-Propanol,1-(isopentyloxy)-3-(2-propynyloxy)-, carbamate (8CI)

Chemical Property of 1-(Isopentyloxy)-3-(2-propynyloxy)-2-propanol carbamate

Chemical Property:

• Vapor Pressure: 9.39E-06mmHg at 25°C
• Boiling Point: 372.8°Cat760mmHg
• Flash Point: 150.7°C
• PSA: 71.77000
• Density: 1.053g/cm³
• LogP: 1.67660

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(Isopentyloxy)-3-(2-propynyloxy)-2-propanol carbamate

There total 4 articles about 1-(Isopentyloxy)-3-(2-propynyloxy)-2-propanol carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

prop-2-ynyloxymethyl-oxirane (18180-30-8) → 1-Propargyloxy-3-isopentyloxy-2-carbamoyloxy-propan (14669-16-0)

Guidance literature:

Multi-step reaction with 2 steps

1: BF₃-Et₂O

2: (i) /BRN= 1098367/, PhNEt₂, toluene, (ii) NH₃

With boron trifluoride diethyl etherate;

Reference yield:

i-Amyl alcohol (123-51-3) → 1-Propargyloxy-3-isopentyloxy-2-carbamoyloxy-propan (14669-16-0)

Guidance literature:

Multi-step reaction with 2 steps

1: BF₃-Et₂O

2: (i) /BRN= 1098367/, PhNEt₂, toluene, (ii) NH₃

With boron trifluoride diethyl etherate;

Reference yield:

phosgene (75-44-5) + 1-(3-methyl-butoxy)-3-prop-2-ynyloxy-propan-2-ol (16169-05-4) → 1-Propargyloxy-3-isopentyloxy-2-carbamoyloxy-propan (14669-16-0)

Guidance literature:

Multistep reaction; (i) /BRN= 1098367/, PhNEt₂, toluene, (ii) NH₃;

upstream raw materials:

phosgene

1-(3-methyl-butoxy)-3-prop-2-ynyloxy-propan-2-ol

prop-2-ynyloxymethyl-oxirane

i-Amyl alcohol