Acetanilide, 2',6'-dibromo-

Base Information

Chemical Name:Acetanilide, 2',6'-dibromo-
CAS No.:33098-80-5
Molecular Formula:C8H7Br2NO
Molecular Weight:292.958
Hs Code.:
DSSTox Substance ID:DTXSID90186761
Nikkaji Number:J54.150H
Wikidata:Q83058146
Mol file:33098-80-5.mol

Synonyms:2,6-Dibromoacetanilide;N-(2,6-dibromophenyl)acetamide;ACETANILIDE, 2',6'-DIBROMO-;33098-80-5;BRN 1818691;0-12-00-00659 (Beilstein Handbook Reference);C8-H7-Br2-N-O;SCHEMBL21807836;DTXSID90186761;Acetamide, N-(2,6-dibromophenyl)-

Suppliers and Price of Acetanilide, 2',6'-dibromo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Acetanilide, 2',6'-dibromo-

Chemical Property:

Vapor Pressure:5.52E-06mmHg at 25°C
Boiling Point:380.3°Cat760mmHg
Flash Point:183.8°C
PSA：32.59000
Density:1.891g/cm³
LogP:3.81950
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:292.88739
Heavy Atom Count:12
Complexity:164

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1=C(C=CC=C1Br)Br

Technology Process of Acetanilide, 2',6'-dibromo-

There total 7 articles about Acetanilide, 2',6'-dibromo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 608-30-0
2,6-dibromoaniline

: 75-36-5
acetyl chloride

: 33098-80-5
N-(2,6-dibromophenyl)acetamide

Guidance literature:: DOI:10.1002/ejoc.200900079

Reference yield:

: 103-84-4
Acetanilid

: 33098-80-5
N-(2,6-dibromophenyl)acetamide

: 614-76-6
N-acetyl-2-bromoaniline

: 103-88-8
4-bromoacetanilide

Guidance literature:: With N-Bromosuccinimide; [Pd(OTs)2(MeCN)2]; toluene-4-sulfonic acid; In toluene; at 20 ℃; for 1h;
DOI:10.1002/anie.201101606

Reference yield:

: 99-09-2
3-nitro-aniline

: 33098-80-5
N-(2,6-dibromophenyl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: concentrated acetic acid; NaOBr

2: glacial acetic acid; NaOBr / 0 °C / man kocht das Reaktionsprodukt mit Essigsaeureanhydrid, trennt die beiden Acetylderivate durch fraktionierte Krystallisation aus Alkohol und verseift sie durch Erhitzen mit konz.Schwefelsaeure auf 120grad

4: bei der Reduktion

5: glacial acetic acid

With sodium hypobromide; acetic acid;