3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, 4-chlorophenyl 2-[[4-[(2,4,5-trichlorophenoxy)carbonyl]phenyl]thio]ethyl ester

Base Information

Chemical Name:3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, 4-chlorophenyl 2-[[4-[(2,4,5-trichlorophenoxy)carbonyl]phenyl]thio]ethyl ester
CAS No.:94119-16-1
Molecular Formula:C₅₁H₄₃Cl₄N₂O₁₁PS
Molecular Weight:1064.76
Hs Code.:

3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-,
4-chlorophenyl 2-[[4-[(2,4,5-trichlorophenoxy)carbonyl]phenyl]thio]ethyl
ester

Synonyms:

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Chemical Property of 3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, 4-chlorophenyl 2-[[4-[(2,4,5-trichlorophenoxy)carbonyl]phenyl]thio]ethyl ester

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Technology Process of 3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, 4-chlorophenyl 2-[[4-[(2,4,5-trichlorophenoxy)carbonyl]phenyl]thio]ethyl ester

There total 4 articles about 3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, 4-chlorophenyl 2-[[4-[(2,4,5-trichlorophenoxy)carbonyl]phenyl]thio]ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1074-36-8
4-mercaptobenzoic acid

: 94119-16-1
5'-O-(4-methoxytrityl)thymidine 3'-(4-chlorophenyl 2-<4-(2,4,5-trichlorophenoxycarbonyl)phenylthio>ethyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: 58.8 percent / Et₃N / dioxane / 40 h / Ambient temperature

2: 61 percent / DCC / dioxane / 15 h

3: 1.) 1,2,4-triazole / 1.) pyridine, 45 min; 2.) pyridine, 4 h

With 1,2,4-Triazole; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1002/hlca.19840670518

Reference yield:

: 7184-99-8
4-((2-hydroxyethyl)thio)benzoic acid

: 94119-16-1
5'-O-(4-methoxytrityl)thymidine 3'-(4-chlorophenyl 2-<4-(2,4,5-trichlorophenoxycarbonyl)phenylthio>ethyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / DCC / dioxane / 15 h

2: 1.) 1,2,4-triazole / 1.) pyridine, 45 min; 2.) pyridine, 4 h

With 1,2,4-Triazole; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1002/hlca.19840670518

Reference yield:

: 7180-09-8
2-(4-carboxyphenylsulphonyl)ethanol

: 94119-16-1
5'-O-(4-methoxytrityl)thymidine 3'-(4-chlorophenyl 2-<4-(2,4,5-trichlorophenoxycarbonyl)phenylthio>ethyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / DCC / dioxane / 15 h

2: 1.) 1,2,4-triazole / 1.) pyridine, 45 min; 2.) pyridine, 4 h

With 1,2,4-Triazole; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1002/hlca.19840670518