CHEMBRDG-BB 5922844

Base Information

• Chemical Name: CHEMBRDG-BB 5922844
• CAS No.: 7184-99-8
• Molecular Formula: C9H10O3S
• Molecular Weight: 198.243
• Hs Code.: 2930909090

Synonyms:<2-Hydroxy-ethylimino>-acetylaceton;4-(2-hydroxyethylimino)pentane-2-one;4-(2-hydroxyethylthio)benzoic acid;2-Pentanone,4-[(2-hydroxyethyl)imino];4-<2-Hydroxy-aethylmercapto>-benzoesaeure;2-(4-carboxyphenylmercapto)ethanol;4-(2-hydroxy-ethylamino)-pent-3-en-2-one;2,4-Pentandion-2-hydroxyethylimin;4-(2-hydroxyethylimino)pent-2-en-2-ol;acetylacetoneethanolimine;acetylacetone mono-{2-hydroxy-ethylimine};4-(2-Hydroxy-ethylsulfanyl)-benzoic acid;

Chemical Property of CHEMBRDG-BB 5922844

Chemical Property:

• PSA: 82.83000
• LogP: 1.46920

Purity/Quality:

98% ^*data from raw suppliers

4-[(2-Hydroxyethyl)thio]benzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHEMBRDG-BB 5922844

There total 6 articles about CHEMBRDG-BB 5922844 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-mercaptobenzoic acid (1074-36-8) + 2-bromoethanol (540-51-2) → 4-((2-hydroxyethyl)thio)benzoic acid (7184-99-8)

Guidance literature:

4-mercaptobenzoic acid; With sodium hydroxide; at 80 ℃; for 0.75h;

2-bromoethanol; for 2h;

With hydrogenchloride; In water;

DOI:10.1039/d0ra00753f

Reference yield: 90.0%

4-mercaptobenzoic acid (1074-36-8) + 2-chloro-ethanol (107-07-3) → 4-((2-hydroxyethyl)thio)benzoic acid (7184-99-8)

Guidance literature:

With sodium hydroxide; at 25 ℃;

DOI:10.1016/S0960-894X(00)00295-X

Reference yield: 58.8%

oxirane (75-21-8,99932-75-9) + 4-mercaptobenzoic acid (1074-36-8) → 4-((2-hydroxyethyl)thio)benzoic acid (7184-99-8)

Guidance literature:

With triethylamine; In 1,4-dioxane; for 40h; Ambient temperature;

DOI:10.1002/hlca.19840670518

upstream raw materials:

oxirane

4-mercaptobenzoic acid

2-chloro-ethanol

2-bromoethanol

Downstream raw materials:

2-<4-(2,4,5-trichlorophenoxycarbonyl)phenylmercapto>ethanol

2-(4-carboxyphenylsulphonyl)ethanol

4-(2-Chloroethylsulfanyl)-benzoic acid

C₃₀H₃₄ClN₉O₄S

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