1-Bromo-2-[(2-methoxyethoxy)methoxy]benzene

Base Information

Chemical Name:1-Bromo-2-[(2-methoxyethoxy)methoxy]benzene
CAS No.:94236-22-3
Molecular Formula:C10H13BrO3
Molecular Weight:261.115
Hs Code.:
DSSTox Substance ID:DTXSID401263514

Synonyms:1-Bromo-2-[(2-methoxyethoxy)methoxy]benzene;DTXSID401263514;94236-22-3

Suppliers and Price of 1-Bromo-2-[(2-methoxyethoxy)methoxy]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Bromo-2-[(2-methoxyethoxy)methoxy]benzene

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:260.00481
Heavy Atom Count:14
Complexity:143

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COCCOCOC1=CC=CC=C1Br

Technology Process of 1-Bromo-2-[(2-methoxyethoxy)methoxy]benzene

There total 1 articles about 1-Bromo-2-[(2-methoxyethoxy)methoxy]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 95-56-7
2-hydroxybromobenzene

: 94236-22-3
1-bromo-2-[(2-methoxyethoxy)methoxy]benzene

Guidance literature:: With triethylamine; In diethyl ether; at 0 ℃;
DOI:10.1016/0040-4039(95)00844-3

Reference yield:

: 94236-22-3
1-bromo-2-[(2-methoxyethoxy)methoxy]benzene

: 205505-72-2
(S)-4-(3-Methoxy-benzyl)-2,2-dimethyl-[1,3]dioxolane-4-carbaldehyde

: 205505-76-6
[(S)-4-(3-Methoxy-benzyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-[2-(2-methoxy-ethoxymethoxy)-phenyl]-methanone

Guidance literature:: With n-butyllithium; sodium acetate; pyridinium chlorochromate; Yield given. Multistep reaction; 1.) THF, -78 deg C to r.t.; 2.) CH₂Cl₂, reflux;
DOI:10.3987/COM-97-S24

Reference yield:

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 94236-22-3
1-bromo-2-[(2-methoxyethoxy)methoxy]benzene

: 167165-56-2
3-bromo-2-(2-methoxyethoxymethoxy)benzaldehyde

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydrogensulfite; Yield given. Multistep reaction; 1.) 0 deg C;
DOI:10.1016/0040-4039(95)00844-3