2-(bromomethyl)-1,3-dichloro-5-methoxybenzene

Base Information

Chemical Name:2-(bromomethyl)-1,3-dichloro-5-methoxybenzene
CAS No.:94278-70-3
Molecular Formula:C8H7BrCl2O
Molecular Weight:269.953
Hs Code.:2916399090
Mol file:94278-70-3.mol

Synonyms:2-bromomethyl-1,3-dichloro-5-methoxy-benzene;2,6-dichloro-4-methoxybenzyl bromide;

Suppliers and Price of 2-(bromomethyl)-1,3-dichloro-5-methoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 2-(bromomethyl)-1,3-dichloro-5-methoxybenzene

Chemical Property:

PSA：9.23000
LogP:3.89690

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(bromomethyl)-1,3-dichloro-5-methoxybenzene

There total 6 articles about 2-(bromomethyl)-1,3-dichloro-5-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82772-93-8
2,6-dichloro-4-methoxy-benzaldehyde

: 94278-70-3
2-(bromomethyl)-1,3-dichloro-5-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 2 h / 7 °C

2: phosphorus tribromide / tetrahydrofuran / 3 h / 0 °C

With sodium tetrahydroborate; phosphorus tribromide; In tetrahydrofuran; ethanol;

Reference yield:

: 60964-09-2
2,6-dichloro-4-hydroxybenzaldehyde

: 94278-70-3
2-(bromomethyl)-1,3-dichloro-5-methoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

2: sodium tetrahydroborate / ethanol / 2 h / 7 °C

3: phosphorus tribromide / tetrahydrofuran / 3 h / 0 °C

With sodium tetrahydroborate; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 94278-65-6
methyl 2,6-dichloro-4-methoxybenzoate

: 94278-70-3
2-(bromomethyl)-1,3-dichloro-5-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / LiAlH₄ / diethyl ether / 3 h / 0 °C

2: 30percent aq. HBr, AcOH / 1.5 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen bromide; acetic acid; In diethyl ether;
DOI:10.1021/jo00203a032