7,8-Dihydro-6-methoxy-6,7-dimethyl-8-(2,4,6-trimethoxyphenyl)-6H-1,3-dioxolo(4,5-g)(1)benzopyran

Base Information

Chemical Name:7,8-Dihydro-6-methoxy-6,7-dimethyl-8-(2,4,6-trimethoxyphenyl)-6H-1,3-dioxolo(4,5-g)(1)benzopyran
CAS No.:116409-16-6
Molecular Formula:C₂₂H₂₆O₇
Molecular Weight:402.444
Hs Code.:
NSC Number:614392
DSSTox Substance ID:DTXSID20922053

Synonyms:116409-16-6;NSC614392;DTXSID20922053;NSC-614392;6H-1,3-Dioxolo(4,5-g)(1)benzopyran, 7,8-dihydro-6-methoxy-6,7-dimethyl-8-(2,4,6-trimethoxyphenyl)-;7,8-Dihydro-6-methoxy-6,7-dimethyl-8-(2,4,6-trimethoxyphenyl)-6H-1,3-dioxolo(4,5-g)(1)benzopyran;6-Methoxy-6,7-dimethyl-8-(2,4,6-trimethoxyphenyl)-7,8-dihydro-2H,6H-[1,3]dioxolo[4,5-g][1]benzopyran

Suppliers and Price of 7,8-Dihydro-6-methoxy-6,7-dimethyl-8-(2,4,6-trimethoxyphenyl)-6H-1,3-dioxolo(4,5-g)(1)benzopyran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7,8-Dihydro-6-methoxy-6,7-dimethyl-8-(2,4,6-trimethoxyphenyl)-6H-1,3-dioxolo(4,5-g)(1)benzopyran

Chemical Property:

Vapor Pressure:4.29E-09mmHg at 25°C
Boiling Point:485.1°Cat760mmHg
Flash Point:193.2°C
Density:1.26g/cm³
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:5
Exact Mass:402.16785316
Heavy Atom Count:29
Complexity:545

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C(C2=CC3=C(C=C2OC1(C)OC)OCO3)C4=C(C=C(C=C4OC)OC)OC

Technology Process of 7,8-Dihydro-6-methoxy-6,7-dimethyl-8-(2,4,6-trimethoxyphenyl)-6H-1,3-dioxolo(4,5-g)(1)benzopyran

There total 5 articles about 7,8-Dihydro-6-methoxy-6,7-dimethyl-8-(2,4,6-trimethoxyphenyl)-6H-1,3-dioxolo(4,5-g)(1)benzopyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67-56-1
methanol

: 116409-15-5
(7R,8R)-6,7-Dimethyl-8-(2,4,6-trimethoxy-phenyl)-7,8-dihydro-6H-[1,3]dioxolo[4,5-g]chromen-6-ol

: 116409-16-6
(7S,8S)-6-Methoxy-6,7-dimethyl-8-(2,4,6-trimethoxy-phenyl)-7,8-dihydro-6H-[1,3]dioxolo[4,5-g]chromene

Guidance literature:: With hydrogen cation;
DOI:10.1002/jhet.5570250113

Reference yield:

: 533-31-3
Sesamol

: 116409-16-6
(7S,8S)-6-Methoxy-6,7-dimethyl-8-(2,4,6-trimethoxy-phenyl)-7,8-dihydro-6H-[1,3]dioxolo[4,5-g]chromene

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / methanol / Heating

2: 95 percent

3: 74 percent / H₃O⁽¹⁺⁾

4: 96 percent / H⁽¹⁺⁾

With oxonium; hydrogen cation; In methanol;
DOI:10.1002/jhet.5570250113

Reference yield:

: 830-79-5
2,4,6-trimethoxybenzaldehyde

: 116409-16-6
(7S,8S)-6-Methoxy-6,7-dimethyl-8-(2,4,6-trimethoxy-phenyl)-7,8-dihydro-6H-[1,3]dioxolo[4,5-g]chromene

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / methanol / Heating

2: 95 percent

3: 74 percent / H₃O⁽¹⁺⁾

4: 96 percent / H⁽¹⁺⁾

With oxonium; hydrogen cation; In methanol;
DOI:10.1002/jhet.5570250113