Naphtho[1,2-c]thiophene-1-carbonitrile, 3-(2,4,6-trimethylphenyl)-

Base Information

Chemical Name:Naphtho[1,2-c]thiophene-1-carbonitrile, 3-(2,4,6-trimethylphenyl)-
CAS No.:94357-65-0
Molecular Formula:C22H17NS
Molecular Weight:327.45
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Naphtho[1,2-c]thiophene-1-carbonitrile, 3-(2,4,6-trimethylphenyl)-

Chemical Property:

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Technology Process of Naphtho[1,2-c]thiophene-1-carbonitrile, 3-(2,4,6-trimethylphenyl)-

There total 3 articles about Naphtho[1,2-c]thiophene-1-carbonitrile, 3-(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 94357-59-2
1-(2,4,6-Trimethyl-phenyl)-3H-2-thia-phenanthrene-4-carbonitrile

: 94357-65-0
1-cyano-3-mesitylnaphtho<1,2-c>thiophene

: 94388-29-1
1-cyano-4-mesityl-2-methoxy-2H-naphtho<1,2-c>thiin

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1246/cl.1984.1973

Reference yield: 34.0%

: 67-56-1
methanol

: 94357-59-2
1-(2,4,6-Trimethyl-phenyl)-3H-2-thia-phenanthrene-4-carbonitrile

: 94357-65-0
1-cyano-3-mesitylnaphtho<1,2-c>thiophene

: 94388-29-1
1-cyano-4-mesityl-2-methoxy-2H-naphtho<1,2-c>thiin

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; 1.) CH₂Cl₂, 0 deg C, 1 h;
DOI:10.1246/cl.1984.1973

Reference yield:

: 87643-55-8
mesityl 2-naphthyl thioketone

: 94357-65-0
1-cyano-3-mesitylnaphtho<1,2-c>thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / Et₃N / 2 h

2: 34 percent / 1.) MCPBA / 1.) CH₂Cl₂, 0 deg C, 1 h

With triethylamine; 3-chloro-benzenecarboperoxoic acid;
DOI:10.1246/cl.1984.1973