(3-amino-6-methyl-4-phenylthieno[2,3-b]pyridin-2-yl)(phenyl)methanone

Base Information

Chemical Name:(3-amino-6-methyl-4-phenylthieno[2,3-b]pyridin-2-yl)(phenyl)methanone
CAS No.:94638-96-7
Molecular Formula:C₂₁H₁₆N₂OS
Molecular Weight:344.437
Hs Code.:

Synonyms:(3-Amino-6-methyl-4-phenyl-thieno[2,3-b]pyridin-2-yl)-phenyl-methanone;3-Amino-2-benzoyl-6-methyl-4-phenylthieno<2,3-b>pyridin;

Suppliers and Price of (3-amino-6-methyl-4-phenylthieno[2,3-b]pyridin-2-yl)(phenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of (3-amino-6-methyl-4-phenylthieno[2,3-b]pyridin-2-yl)(phenyl)methanone

Chemical Property:

Melting Point:151 - 153 °C (ethanol)
PSA：84.22000
LogP:5.66610

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3-amino-6-methyl-4-phenylthieno[2,3-b]pyridin-2-yl)(phenyl)methanone

There total 7 articles about (3-amino-6-methyl-4-phenylthieno[2,3-b]pyridin-2-yl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 78564-23-5
6-methyl-4-phenyl-2-thioxo-1,2-dihydropyridine-3-carbonitrile

: 70-11-1
α-bromoacetophenone

: 94638-96-7
(3-amino-6-methyl-4-phenyl-thieno[2,3-b]pyridin-2-yl)-phenyl-methanone

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; for 4h;

Reference yield:

: 96539-80-9
6-Methyl-2-(2-oxo-2-phenyl-ethylsulfanyl)-4-phenyl-nicotinonitrile

: 94638-96-7
(3-amino-6-methyl-4-phenyl-thieno[2,3-b]pyridin-2-yl)-phenyl-methanone

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 5h; Yield given;
DOI:10.1007/BF00960275

Reference yield:

: 2700-22-3
Benzylidenemalononitrile

: 94638-96-7
(3-amino-6-methyl-4-phenyl-thieno[2,3-b]pyridin-2-yl)-phenyl-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / Et₂NH / methanol / 120 h / 20 - 25 °C

2: 82 percent / 10percent KOH / dimethylformamide / 4 h

With potassium hydroxide; diethylamine; In methanol; N,N-dimethyl-formamide;