3-Nitroso-2-phenylimidazo[1,2-a]pyrimidine

Base Information

Chemical Name:3-Nitroso-2-phenylimidazo[1,2-a]pyrimidine
CAS No.:28103-25-5
Molecular Formula:C12H8 N4 O
Molecular Weight:224.2181
Hs Code.:
NSC Number:77443
UNII:MB84EN3PTV
DSSTox Substance ID:DTXSID90182384
Nikkaji Number:J374.508B
Wikidata:Q27147587
Mol file:28103-25-5.mol

Synonyms:3-Nitroso-2-phenylimidazo[1,2-a]pyrimidine;28103-25-5;3-Nitroso-2-phenylimidazo(1,2-a)pyrimidine;MB84EN3PTV;NSC 77443;NSC77443;UNII-MB84EN3PTV;NSC-77443;2-phenyl-3-nitrosoimidazo[1,2-a]pyrimidine;NCIOpen2_004118;SCHEMBL3787920;CHEBI:78015;DTXSID90182384;STL417065;AKOS000416767;3-nitroso-2-phenyl-imidazo[1,2-a]pyrimidine;Q27147587;IMIDAZO(1,2-A)PYRIMIDINE, 3-NITROSO-2-PHENYL-

Suppliers and Price of 3-Nitroso-2-phenylimidazo[1,2-a]pyrimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 3-Nitroso-2-phenylimidazo[1,2-a]pyrimidine

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.37g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:224.06981089
Heavy Atom Count:17
Complexity:280

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(N3C=CC=NC3=N2)N=O

Technology Process of 3-Nitroso-2-phenylimidazo[1,2-a]pyrimidine

There total 6 articles about 3-Nitroso-2-phenylimidazo[1,2-a]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1-(2-Imino-2H-pyrazin-1-yl)-2-phenyl-ethane-1,2-dione 1-oxime

: 28103-25-5
2-phenyl-3-nitrosoimidazo[1,2-a]pyrimidine

Guidance literature:: With sodium nitrite; In water; acetic acid; for 24h;

Reference yield:

: 15764-47-3
2-phenylimidazo(1,2-a)pyrimidine

: 28103-25-5
2-phenyl-3-nitrosoimidazo[1,2-a]pyrimidine

Guidance literature:: With acetic acid; sodium nitrite;
DOI:10.1016/0223-5234(91)90208-5

Reference yield:

: 70-11-1
α-bromoacetophenone

: 28103-25-5
2-phenyl-3-nitrosoimidazo[1,2-a]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-dimethoxy-ethane / 48 h / Heating

2: NaNO₂, AcOH

With acetic acid; sodium nitrite; In 1,2-dimethoxyethane;
DOI:10.1016/0223-5234(91)90208-5