Trisulfide, methyl phenylmethyl

Base Information

• Chemical Name: Trisulfide, methyl phenylmethyl
• CAS No.: 94839-55-1
• Molecular Formula: C8H10S3
• Molecular Weight: 202.365
• Mol file: 94839-55-1.mol

Synonyms:

Chemical Property of Trisulfide, methyl phenylmethyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Trisulfide, methyl phenylmethyl

There total 5 articles about Trisulfide, methyl phenylmethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

Methoxycarbonylmethyl trisulfane (94839-60-8) + phenylmethanethiol (100-53-8) → 1-benzyl-2-methyldisulfide (699-10-5) + Methyl benzyl trisulfane (94839-55-1)

Guidance literature:

4-methyl-morpholine; In chloroform; at 25 ℃; for 4h;

DOI:10.1055/s-1984-30922

Reference yield:

dibenzyl disulphide (150-60-7) + methanethiosulfonic acid S-methyl ester (2949-92-0,31761-75-8) → dibenzyltrisulfide (6493-73-8) + 1-benzyl-2-methyldisulfide (699-10-5) + Methyl benzyl trisulfane (94839-55-1)

Guidance literature:

With sodium sulfide; In aq. phosphate buffer; water; dimethyl sulfoxide; at 20 ℃; for 0.5h;

DOI:10.1002/anie.201704117

Reference yield:

methanethiosulfonic acid S-methyl ester (2949-92-0,31761-75-8) + BW-HP-205 → Methyl benzyl trisulfane (94839-55-1)

Guidance literature:

With porcine liver esterase; In aq. phosphate buffer; dimethyl sulfoxide; at 20 ℃; for 0.166667h; Enzymatic reaction;

DOI:10.1002/anie.201704117

upstream raw materials:

methylthiol

acetyl benzyl disulfide

Methoxycarbonylmethyl trisulfane

phenylmethanethiol

Refernces

• 1、 Mott, Andrew W.,Barany, George. "A New Method for the Synthesis of Unsymmetrical Trisulfanes". . p. 657 - 660. Retrieved 2007/10/02.