1H-Pyrazole-4,5-dicarboxylic acid, 1-[2-[(2-methyl-2-propenyl)thio]phenyl]-3-(4-nitrophenyl)-, dimethyl ester

Base Information

Chemical Name:1H-Pyrazole-4,5-dicarboxylic acid, 1-[2-[(2-methyl-2-propenyl)thio]phenyl]-3-(4-nitrophenyl)-, dimethyl ester
CAS No.:95065-86-4
Molecular Formula:C₂₃H₂₁N₃O₆S
Molecular Weight:467.502
Hs Code.:

Synonyms:

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Chemical Property of 1H-Pyrazole-4,5-dicarboxylic acid, 1-[2-[(2-methyl-2-propenyl)thio]phenyl]-3-(4-nitrophenyl)-, dimethyl ester

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Technology Process of 1H-Pyrazole-4,5-dicarboxylic acid, 1-[2-[(2-methyl-2-propenyl)thio]phenyl]-3-(4-nitrophenyl)-, dimethyl ester

There total 5 articles about 1H-Pyrazole-4,5-dicarboxylic acid, 1-[2-[(2-methyl-2-propenyl)thio]phenyl]-3-(4-nitrophenyl)-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37845-59-3
2-[(2-methyl-2-propenyl)thio]benzamine

: 95065-86-4
2-[2-(2-Methyl-allylsulfanyl)-phenyl]-5-(4-nitro-phenyl)-2H-pyrazole-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium nitrite, 1M-hydrochloric acid, 2.) sodium acetate / 1.) water, 0 deg C, 2.) 70percent aq. methanol, room temperature, 3 h

2: 67 percent / triethylamine / acetonitrile / 0.67 h / Ambient temperature

3: 0.16 g / dimethyl acetylenedicarboxylate / benzene / 168 h / Heating

With hydrogenchloride; sodium acetate; triethylamine; dimethyl acetylenedicarboxylate; sodium nitrite; In acetonitrile; benzene;

Reference yield:

: 95065-76-2
C₁₇H₁₆ClN₃O₂S

: 95065-86-4
2-[2-(2-Methyl-allylsulfanyl)-phenyl]-5-(4-nitro-phenyl)-2H-pyrazole-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / triethylamine / acetonitrile / 0.67 h / Ambient temperature

2: 0.16 g / dimethyl acetylenedicarboxylate / benzene / 168 h / Heating

With triethylamine; dimethyl acetylenedicarboxylate; In acetonitrile; benzene;

Reference yield:

: 23022-79-9
1-chloro-1-(4-nitrophenyl)propan-2-one

: 95065-86-4
2-[2-(2-Methyl-allylsulfanyl)-phenyl]-5-(4-nitro-phenyl)-2H-pyrazole-3,4-dicarboxylic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium nitrite, 1M-hydrochloric acid, 2.) sodium acetate / 1.) water, 0 deg C, 2.) 70percent aq. methanol, room temperature, 3 h

2: 67 percent / triethylamine / acetonitrile / 0.67 h / Ambient temperature

3: 0.16 g / dimethyl acetylenedicarboxylate / benzene / 168 h / Heating

With hydrogenchloride; sodium acetate; triethylamine; dimethyl acetylenedicarboxylate; sodium nitrite; In acetonitrile; benzene;