2-(Benzenesulfinyl)-2-cyclohexyl-1-oxaspiro[2.5]octane

Base Information

Chemical Name:2-(Benzenesulfinyl)-2-cyclohexyl-1-oxaspiro[2.5]octane
CAS No.:95110-49-9
Molecular Formula:C19H26O2S
Molecular Weight:318.48
Hs Code.:
DSSTox Substance ID:DTXSID90537996

Synonyms:95110-49-9;2-(Benzenesulfinyl)-2-cyclohexyl-1-oxaspiro[2.5]octane;DTXSID90537996

Suppliers and Price of 2-(Benzenesulfinyl)-2-cyclohexyl-1-oxaspiro[2.5]octane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(Benzenesulfinyl)-2-cyclohexyl-1-oxaspiro[2.5]octane

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:318.16535124
Heavy Atom Count:22
Complexity:417

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)C2(C3(O2)CCCCC3)S(=O)C4=CC=CC=C4

Technology Process of 2-(Benzenesulfinyl)-2-cyclohexyl-1-oxaspiro[2.5]octane

There total 7 articles about 2-(Benzenesulfinyl)-2-cyclohexyl-1-oxaspiro[2.5]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102104-37-0
1-(Benzenesulfinyl-chloro-cyclohexyl-methyl)-cyclohexanol

: 95110-49-9
2'-cyclohexyl-2'-phenylsulfinylspiro

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; tert-butyl alcohol; Ambient temperature;
DOI:10.1246/bcsj.64.1129

Reference yield:

: 104354-60-1
cyclohexylchloromethyl phenyl sulfoxide

: 95110-49-9
2'-cyclohexyl-2'-phenylsulfinylspiro

Guidance literature:: Multi-step reaction with 2 steps

1: 1) lithium diisopropylamide / 1) THF, -70 deg C, 20 min, 2) THF, -70 deg C, 10 min

2: 30percent aq. KOH / methanol / 1 h / Ambient temperature

With potassium hydroxide; lithium diisopropyl amide; In methanol;
DOI:10.1246/bcsj.58.1983

Reference yield:

: 13307-61-4
Isobutylthiobenzene

: 95110-49-9
2'-cyclohexyl-2'-phenylsulfinylspiro

Guidance literature:: Multi-step reaction with 4 steps

1: N-chlorosuccinimide / CCl₄ / 2.5 h / Ambient temperature

2: m-chloroperoxybenzoic acid / CH₂Cl₂ / -60 - -40 °C

3: 1) lithium diisopropylamide / 1) THF, -70 deg C, 20 min, 2) THF, -70 deg C, 10 min

4: 30percent aq. KOH / methanol / 1 h / Ambient temperature

With potassium hydroxide; N-chloro-succinimide; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In methanol; tetrachloromethane; dichloromethane;
DOI:10.1246/bcsj.58.1983