Methanone, 1-cyclohexen-1-ylcyclohexyl-

Base Information

Chemical Name:Methanone, 1-cyclohexen-1-ylcyclohexyl-
CAS No.:74598-74-6
Molecular Formula:C13H20O
Molecular Weight:192.301
Hs Code.:

Synonyms:cyclohex-1-enyl-cyclohexyl ketone;Methanone,1-cyclohexen-1-ylcyclohexyl;Cyclohex-1-enyl-cyclohexyl-keton;

Suppliers and Price of Methanone, 1-cyclohexen-1-ylcyclohexyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Cyclohexyl-1-cyclohexenylKetone
2.5g
$ 1130.00

AK Scientific
Methanone,1-cyclohexen-1-ylcyclohexyl-
10g
$ 2997.00

A2B
(cyclohex-1-en-1-yl)(cyclohexyl)methanone 95.0%
1g
$ 544.00

A2B
(cyclohex-1-en-1-yl)(cyclohexyl)methanone 95.0%
500mg
$ 419.00

A2B
(cyclohex-1-en-1-yl)(cyclohexyl)methanone 95.0%
250mg
$ 245.00

A2B
(cyclohex-1-en-1-yl)(cyclohexyl)methanone 95.0%
100mg
$ 185.00

Total 6 raw suppliers

Chemical Property of Methanone, 1-cyclohexen-1-ylcyclohexyl-

Chemical Property:

Melting Point:176-177 °C
Boiling Point:152-153 °C(Press: 14 Torr)
PSA：17.07000
Density:1.004±0.06 g/cm3(Predicted)
LogP:3.63620

Purity/Quality:

99% ^*data from raw suppliers

Cyclohexyl-1-cyclohexenylKetone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Cyclohexyl-1-cyclohexenyl Ketone is used in the preparation of enones by nickel-catalyzed carbonylative Negishi cross-coupling.

Technology Process of Methanone, 1-cyclohexen-1-ylcyclohexyl-

There total 17 articles about Methanone, 1-cyclohexen-1-ylcyclohexyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 201230-82-2
carbon monoxide

: 28075-50-5
cyclohex-1-en-1-yl trifluoromethane sulfonate

: 931-51-1
cyclohexylmagnesiumchloride

: 74598-74-6
cyclohex-1-en-1-yl(cyclohexyl)methanone

Guidance literature:: cyclohexylmagnesiumchloride; With zinc(II) chloride; In tetrahydrofuran; at 20 ℃;

carbon monoxide; cyclohex-1-en-1-yl trifluoromethane sulfonate; With magnesium bromide; nickel dichloride; In tetrahydrofuran; dimethyl sulfoxide; at 80 ℃; for 0.333333h; under 760.051 Torr; Further stages.;
DOI:10.1016/j.tetlet.2008.03.035

Reference yield: 83.0%

: 95110-49-9
2'-cyclohexyl-2'-phenylsulfinylspiro

: 74598-74-6
cyclohex-1-en-1-yl(cyclohexyl)methanone

Guidance literature:: With Tributylphosphine oxide; lithium perchlorate; In toluene; for 0.833333h; Heating;
DOI:10.1246/bcsj.60.1839

Reference yield: 67.0%

: 1977-87-3
cyclohexanecarbonyl fluoride

: 28075-50-5
cyclohex-1-en-1-yl trifluoromethane sulfonate

: 74598-74-6
cyclohex-1-en-1-yl(cyclohexyl)methanone

Guidance literature:: With 2,2':6,2''-terpyridine; manganese; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; In N,N-dimethyl acetamide; toluene; at 70 ℃; for 15h; Sealed tube;
DOI:10.1021/acs.orglett.9b01164