Technology Process of 1-Cyclohexyl-1-(1,2-epoxycyclohexyl)ethylene
There total 6 articles about 1-Cyclohexyl-1-(1,2-epoxycyclohexyl)ethylene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) lithium diisopropylamide / 1.) THF, -60 deg C, 2.) -60 deg C
2: t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran / Ambient temperature
3: LiClO4*3H2O, tributylphosphine oxide / toluene / Heating
4: 30 percent H2O2, KOH / methanol / Ambient temperature
5: 1.) t-BuOK / 1.) THF, r.t., 2.) r.t.
With
potassium hydroxide; Tributylphosphine oxide; potassium tert-butylate; dihydrogen peroxide; lithium perchlorate; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; toluene; tert-butyl alcohol;
DOI:10.1246/bcsj.64.1129
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) lithium diisopropylamide / 1.) THF, -60 deg C, 2.) -60 deg C
2: t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran / Ambient temperature
3: LiClO4*3H2O, tributylphosphine oxide / toluene / Heating
4: 30 percent H2O2, KOH / methanol / Ambient temperature
5: 1.) t-BuOK / 1.) THF, r.t., 2.) r.t.
With
potassium hydroxide; Tributylphosphine oxide; potassium tert-butylate; dihydrogen peroxide; lithium perchlorate; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; toluene; tert-butyl alcohol;
DOI:10.1246/bcsj.64.1129
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 30 percent H2O2, KOH / methanol / Ambient temperature
2: 1.) t-BuOK / 1.) THF, r.t., 2.) r.t.
With
potassium hydroxide; potassium tert-butylate; dihydrogen peroxide;
In
methanol;
DOI:10.1246/bcsj.64.1129
