1,4-Benzenediol, 2-[10-(acetyloxy)decyl]-5,6-dimethoxy-3-methyl-, 4-(hydrogen sulfate), monosodium salt

Base Information

• Chemical Name: 1,4-Benzenediol, 2-[10-(acetyloxy)decyl]-5,6-dimethoxy-3-methyl-, 4-(hydrogen sulfate), monosodium salt
• CAS No.: 95233-57-1
• Molecular Formula: C₂₁H₃₃O₉S*Na
• Molecular Weight: 484.543

Synonyms:

Chemical Property of 1,4-Benzenediol, 2-[10-(acetyloxy)decyl]-5,6-dimethoxy-3-methyl-, 4-(hydrogen sulfate), monosodium salt

Chemical Property:

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Technology Process of 1,4-Benzenediol, 2-[10-(acetyloxy)decyl]-5,6-dimethoxy-3-methyl-, 4-(hydrogen sulfate), monosodium salt

There total 3 articles about 1,4-Benzenediol, 2-[10-(acetyloxy)decyl]-5,6-dimethoxy-3-methyl-, 4-(hydrogen sulfate), monosodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Idebenone (58186-27-9) → C21H33O9S(1-)*Na(1+) (95233-57-1)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine

2: 10 percent sodium hydrosulfite / diethyl ether

3: 1.) chlorosulfonic acid, sodium hydrosulfite; 2.) NaOH / pyridine / 2.) pH = 8-9

With chlorosulfonic acid; sodium hydroxide; sodium disulfite; In pyridine; diethyl ether;

DOI:10.1248/cpb.33.3756

Reference yield:

2,3-dimethoxy-5-methyl-6-(10'-acetoxydecyl)-1,4-benzoquinone (58186-28-0) → C21H33O9S(1-)*Na(1+) (95233-57-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 10 percent sodium hydrosulfite / diethyl ether

2: 1.) chlorosulfonic acid, sodium hydrosulfite; 2.) NaOH / pyridine / 2.) pH = 8-9

With chlorosulfonic acid; sodium hydroxide; sodium disulfite; In pyridine; diethyl ether;

DOI:10.1248/cpb.33.3756

Reference yield:

6-(10-Acetoxydecyl)-2,3-dimethoxy-5-methylhydroquinone (95233-55-9) → C21H33O9S(1-)*Na(1+) (95233-56-0) + C21H33O9S(1-)*Na(1+) (95233-57-1) + C21H32O12S2(2-)*2Na(1+) (95233-58-2)

Guidance literature:

With chlorosulfonic acid; sodium disulfite; In pyridine; 2.) pH = 8-9;

DOI:10.1248/cpb.33.3756

upstream raw materials:

6-(10-Acetoxydecyl)-2,3-dimethoxy-5-methylhydroquinone

Idebenone

2,3-dimethoxy-5-methyl-6-(10'-acetoxydecyl)-1,4-benzoquinone

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