(1E)-1-(1-benzylimidazolidin-2-ylidene)propan-2-one

Base Information

Chemical Name:(1E)-1-(1-benzylimidazolidin-2-ylidene)propan-2-one
CAS No.:95271-72-0
Molecular Formula:C₁₃H₁₆N₂O
Molecular Weight:216.283
Hs Code.:
DSSTox Substance ID:DTXSID301151958
Nikkaji Number:J1.711.128K

Synonyms:DTXSID301151958;95271-72-0;1-Propen-2-ol, 1-[4,5-dihydro-1-(phenylmethyl)-1H-imidazol-2-yl]-, (Z)-

Suppliers and Price of (1E)-1-(1-benzylimidazolidin-2-ylidene)propan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (1E)-1-(1-benzylimidazolidin-2-ylidene)propan-2-one

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:216.126263138
Heavy Atom Count:16
Complexity:280

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C=C1NCCN1CC2=CC=CC=C2
Isomeric SMILES:CC(=O)/C=C/1\NCCN1CC2=CC=CC=C2

Technology Process of (1E)-1-(1-benzylimidazolidin-2-ylidene)propan-2-one

There total 3 articles about (1E)-1-(1-benzylimidazolidin-2-ylidene)propan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 6096-36-2
1-benzyl-2-methyl-4,5-dihydro-1H-imidazole

: 141-78-6
ethyl acetate

: 95271-72-0
1-benzyl-2-(2-hydroxyprop-1-enyl)-4,5-dihydroimidazole

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 1 h, 2.) -78 to 20 deg C, 1 h, 3.) 20 deg C, 16 h;

Reference yield:

: 95271-71-9
1-benzyl-2-methyl-4,5-dihydroimidazole hydrochloride

: 95271-72-0
1-benzyl-2-(2-hydroxyprop-1-enyl)-4,5-dihydroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 35 g / 30percent aq. sodium hydroxide

2: 72 percent / n-butyl-lithium / hexane; tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) -78 to 20 deg C, 1 h, 3.) 20 deg C, 16 h

With sodium hydroxide; n-butyllithium; In tetrahydrofuran; hexane;

Reference yield:

: 4152-09-4
N-benzylethylenediamine

: 95271-72-0
1-benzyl-2-(2-hydroxyprop-1-enyl)-4,5-dihydroimidazole

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 3 h / Heating

2: 35 g / 30percent aq. sodium hydroxide

3: 72 percent / n-butyl-lithium / hexane; tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) -78 to 20 deg C, 1 h, 3.) 20 deg C, 16 h

With sodium hydroxide; n-butyllithium; In tetrahydrofuran; ethanol; hexane;