Technology Process of Silane,
(1,1-dimethylethyl)[2-[3-(2,2-dimethyl-6-methylenecyclohexyl)propyl]-1,3
-dithian-2-yl]dimethyl-
There total 6 articles about Silane,
(1,1-dimethylethyl)[2-[3-(2,2-dimethyl-6-methylenecyclohexyl)propyl]-1,3
-dithian-2-yl]dimethyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane;
for 2.5h;
Ambient temperature;
DOI:10.1002/hlca.19840670711
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1) I2, 2) 2N NaOH / 1) pyridine, 100 deg C, 1 h; 2) 100 deg C, overnight
2: 88 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature
3: 81 percent / pyridine / 0.08 h / Ambient temperature
4: 96 percent / NaI / 1,2-dimethoxy-ethane / 18 h / 50 °C
5: 92 percent / BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 2.5 h / Ambient temperature
With
pyridine; sodium hydroxide; lithium aluminium tetrahydride; n-butyllithium; iodine; sodium iodide;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; diethyl ether; hexane;
DOI:10.1002/hlca.19840670711
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 81 percent / pyridine / 0.08 h / Ambient temperature
2: 96 percent / NaI / 1,2-dimethoxy-ethane / 18 h / 50 °C
3: 92 percent / BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 2.5 h / Ambient temperature
With
pyridine; n-butyllithium; sodium iodide;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; hexane;
DOI:10.1002/hlca.19840670711
