Propanedioic acid, [[1-[1-hydroxy-2-[(4-nitrophenyl)methoxy]-2-oxoethyl]-4-oxo-3-[(phenoxy acetyl)amino]-2-azetidinyl]thio]-, methyl (4-nitrophenyl)methyl ester

Base Information

Chemical Name:Propanedioic acid, [[1-[1-hydroxy-2-[(4-nitrophenyl)methoxy]-2-oxoethyl]-4-oxo-3-[(phenoxy acetyl)amino]-2-azetidinyl]thio]-, methyl (4-nitrophenyl)methyl ester
CAS No.:95477-36-4
Molecular Formula:C₃₁H₂₈N₄O₁₄S
Molecular Weight:712.648
Hs Code.:

Propanedioic acid,
[[1-[1-hydroxy-2-[(4-nitrophenyl)methoxy]-2-oxoethyl]-4-oxo-3-[(phenoxy
acetyl)amino]-2-azetidinyl]thio]-, methyl (4-nitrophenyl)methyl ester

Synonyms:

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Chemical Property of Propanedioic acid, [[1-[1-hydroxy-2-[(4-nitrophenyl)methoxy]-2-oxoethyl]-4-oxo-3-[(phenoxy acetyl)amino]-2-azetidinyl]thio]-, methyl (4-nitrophenyl)methyl ester

Chemical Property:

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Technology Process of Propanedioic acid, [[1-[1-hydroxy-2-[(4-nitrophenyl)methoxy]-2-oxoethyl]-4-oxo-3-[(phenoxy acetyl)amino]-2-azetidinyl]thio]-, methyl (4-nitrophenyl)methyl ester

There total 4 articles about Propanedioic acid, [[1-[1-hydroxy-2-[(4-nitrophenyl)methoxy]-2-oxoethyl]-4-oxo-3-[(phenoxy acetyl)amino]-2-azetidinyl]thio]-, methyl (4-nitrophenyl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Malonic acid methyl ester 4-nitro-benzyl ester

: 95477-36-4
2-[1-[Hydroxy-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / NaH / tetrahydrofuran / 0.75 h / 0 °C

With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)91387-5

Reference yield:

: 73395-53-6
N-[2-(Benzothiazol-2-yldisulfanyl)-4-oxo-azetidin-3-yl]-2-phenoxy-acetamide

: 95477-36-4
2-[1-[Hydroxy-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / NaH / tetrahydrofuran / 0.75 h / 0 °C

With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)91387-5

Reference yield:

: 75283-03-3
2-[2-(Benzothiazol-2-yldisulfanyl)-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-1-yl]-3-methyl-but-2-enoic acid methyl ester

: 95477-36-4
2-[1-[Hydroxy-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1., ozonolysis; 2., treatment with methanol

2: 78 percent / NaH / tetrahydrofuran / 0.75 h / 0 °C

With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)91387-5