2-[1-[Chloro-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

Base Information

Chemical Name:2-[1-[Chloro-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester
CAS No.:95477-39-7
Molecular Formula:C₃₁H₂₇ClN₄O₁₃S
Molecular Weight:731.093
Hs Code.:

2-[1-[Chloro-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

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Chemical Property of 2-[1-[Chloro-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

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Technology Process of 2-[1-[Chloro-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

There total 6 articles about 2-[1-[Chloro-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Malonic acid methyl ester 4-nitro-benzyl ester

: 95477-39-7
2-[1-[Chloro-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaH / tetrahydrofuran / 0.75 h / 0 °C

3: thionyl chloride

With thionyl chloride; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)91387-5

Reference yield:

: 73395-53-6
N-[2-(Benzothiazol-2-yldisulfanyl)-4-oxo-azetidin-3-yl]-2-phenoxy-acetamide

: 95477-39-7
2-[1-[Chloro-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaH / tetrahydrofuran / 0.75 h / 0 °C

3: thionyl chloride

With thionyl chloride; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)91387-5

Reference yield:

: 75283-03-3
2-[2-(Benzothiazol-2-yldisulfanyl)-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-1-yl]-3-methyl-but-2-enoic acid methyl ester

: 95477-39-7
2-[1-[Chloro-(4-nitro-benzyloxycarbonyl)-methyl]-4-oxo-3-(2-phenoxy-acetylamino)-azetidin-2-ylsulfanyl]-malonic acid methyl ester 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1., ozonolysis; 2., treatment with methanol

2: 78 percent / NaH / tetrahydrofuran / 0.75 h / 0 °C

4: thionyl chloride

With thionyl chloride; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)91387-5