3,4-Dimethoxybenzene-1-sulfonyl fluoride

Base Information

Chemical Name:3,4-Dimethoxybenzene-1-sulfonyl fluoride
CAS No.:95546-50-2
Molecular Formula:C₈H₉FO₄S
Molecular Weight:220.221
Hs Code.:
European Community (EC) Number:809-782-5

Synonyms:3,4-dimethoxybenzene-1-sulfonyl fluoride;95546-50-2;3,4-DIMETHOXYBENZENESULFONYL FLUORIDE;3,4-dimethoxybenzene-1-sulfonylfluoride;AKOS022542768;VS-0081;3,4-Dimethoxybenzenesulfonyl fluoride, 95%;EN300-728607;F72595

Suppliers and Price of 3,4-Dimethoxybenzene-1-sulfonyl fluoride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 6 raw suppliers

Chemical Property of 3,4-Dimethoxybenzene-1-sulfonyl fluoride

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:220.02055810
Heavy Atom Count:14
Complexity:272

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)S(=O)(=O)F)OC

Technology Process of 3,4-Dimethoxybenzene-1-sulfonyl fluoride

There total 3 articles about 3,4-Dimethoxybenzene-1-sulfonyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 23095-31-0
3,4-dimethoxybenzene-1-sulfonyl chloride

: 95546-50-2
3,4-dimethoxybenzenesulfonyl fluoride

Guidance literature:: With tri-n-propylamine; fluorosulfonyl fluoride; In acetone; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2022.132657

Reference yield: 40.0%

: 100886-20-2
1,2-dimethoxy-4-phenoxybenzene

: 95546-50-2
3,4-dimethoxybenzenesulfonyl fluoride

Guidance literature:: With fluorosulphonic acid; at 0 ℃; for 1.5h;

Reference yield:

: 6315-89-5
3,4-dimethoxyaniline

: 95546-50-2
3,4-dimethoxybenzenesulfonyl fluoride

Guidance literature:: 3,4-dimethoxyaniline; With tetrafluoroboric acid; tert.-butylnitrite; In ethanol; water; at 0 - 20 ℃; for 1h;

With 6,6'-dimethyl-2,2'-bipyridine; potassium hydrogen difluoride; 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate; copper dichloride; In acetonitrile; at 20 ℃; for 12h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.0c00484