2-[4-(Dimethylamino)phenyl]-4H-3,1-benzoxazin-4-one

Base Information

Chemical Name:2-[4-(Dimethylamino)phenyl]-4H-3,1-benzoxazin-4-one
CAS No.:95654-38-9
Molecular Formula:C16H14N2O2
Molecular Weight:266.299
Hs Code.:
DSSTox Substance ID:DTXSID10537251
Nikkaji Number:J2.998.372K
Wikidata:Q82412195

Synonyms:95654-38-9;2-[4-(Dimethylamino)phenyl]-4H-3,1-benzoxazin-4-one;DTXSID10537251

Suppliers and Price of 2-[4-(Dimethylamino)phenyl]-4H-3,1-benzoxazin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[4-(Dimethylamino)phenyl]-4H-3,1-benzoxazin-4-one

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:266.105527694
Heavy Atom Count:20
Complexity:397

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=CC=C(C=C1)C2=NC3=CC=CC=C3C(=O)O2

Technology Process of 2-[4-(Dimethylamino)phenyl]-4H-3,1-benzoxazin-4-one

There total 7 articles about 2-[4-(Dimethylamino)phenyl]-4H-3,1-benzoxazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 201230-82-2
carbon monoxide

: 586-77-6
4-bromo-N,N-dimethylaniline

: 615-36-1
2-bromoaniline

: 95654-38-9
2-(4-(dimethylamino)phenyl)-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: With palladium diacetate; N-ethyl-N,N-diisopropylamine; catacxium A; In toluene; at 110 ℃; for 20h; under 3750.38 Torr; chemoselective reaction; Inert atmosphere; Autoclave;
DOI:10.1002/chem.201102254

Reference yield: 64.0%

: 1-(4-N,N-dimethylaminobenzoyl)benzotriazole

: 201230-82-2
carbon monoxide

: 95654-38-9
2-(4-(dimethylamino)phenyl)-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: With silver trifluoromethanesulfonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium dichloride; In acetonitrile; at 120 ℃; for 16h; under 30003 Torr; Inert atmosphere; Autoclave;
DOI:10.1021/acs.orglett.7b03184