o-(p-(Dimethylamino)benzylideneamino)phenol

Base Information

• Chemical Name: o-(p-(Dimethylamino)benzylideneamino)phenol
• CAS No.: 3230-43-1
• Molecular Formula: C₁₅H₁₆N₂O
• Molecular Weight: 240.305
• European Community (EC) Number: 653-013-4
• NSC Number: 112118
• DSSTox Substance ID: DTXSID20296842
• Nikkaji Number: J882.929B
• Wikidata: Q82037629
• ChEMBL ID: CHEMBL2236145
• Mol file: 3230-43-1.mol

Synonyms:3230-43-1;o-(p-(Dimethylamino)benzylideneamino)phenol;2-[[4-(dimethylamino)phenyl]methylideneamino]phenol;2-[(4-DIMETHYLAMINO-BENZYLIDENE)-AMINO]-PHENOL;2-({(E)-[4-(dimethylamino)phenyl]methylidene}amino)phenol;(E)-2-((4-(dimethylamino)benzylidene)amino)phenol;NSC112118;CHEMBL2236145;SCHEMBL10415405;DTXSID20296842;GJZBNSJPZKCNPU-LFIBNONCSA-N;BBL027856;STK833471;AKOS003614900;AKOS024333358;NSC-112118;VS-08604;2-[4-(Dimethylamino)benzylideneimino]phenol;2-hydroxy-N-(4'-dimethylaminobenzylidene)aniline;2-(((E)-[4-(Dimethylamino)phenyl]methylidene)amino)phenol #;2-({[4-(DIMETHYLAMINO)PHENYL]METHYLIDENE}AMINO)PHENOL;2-[(E)-{[4-(DIMETHYLAMINO)PHENYL]METHYLIDENE}AMINO]PHENOL

Chemical Property of o-(p-(Dimethylamino)benzylideneamino)phenol

Chemical Property:

• Vapor Pressure: 6.43E-08mmHg at 25°C
• Boiling Point: 427.7°Cat760mmHg
• Flash Point: 212.5°C
• PSA: 35.83000
• Density: 1.05g/cm³
• LogP: 3.20880
• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 240.126263138
• Heavy Atom Count: 18
• Complexity: 270

Purity/Quality:

99% ^*data from raw suppliers

(E)-2-((4-(DIMETHYLAMINO)BENZYLIDENE)AMINO)PHENOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)C=NC2=CC=CC=C2O

Technology Process of o-(p-(Dimethylamino)benzylideneamino)phenol

There total 4 articles about o-(p-(Dimethylamino)benzylideneamino)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-amino-phenol (95-55-6) + 4-dimethylamino-benzaldehyde (100-10-7) → 2-(4-dimethylamino-benzylidenamino)-phenol (1624-49-3,3230-43-1)

Guidance literature:

In ethanol; at 25 ℃; for 24h;

DOI:10.1016/j.tet.2016.12.026

Reference yield:

2-(N,N-dimethyl-4-aminophenyl)acetaldehyde (99074-89-2) + 2-amino-phenol (95-55-6) → 2-(4-dimethylamino-benzylidenamino)-phenol (1624-49-3,3230-43-1)

Guidance literature:

In methanol; Ambient temperature;

Reference yield:

ethanol (64-17-5) + water (7732-18-5) + 2-amino-phenol (95-55-6) + 4-dimethylamino-benzaldehyde (100-10-7) → 2-(4-dimethylamino-benzylidenamino)-phenol (1624-49-3,3230-43-1)

Guidance literature:

upstream raw materials:

2-amino-phenol

4-dimethylamino-benzaldehyde

2-(N,N-dimethyl-4-aminophenyl)acetaldehyde

ethanol

Downstream raw materials:

N-(2-hydroxy-phenyl)-toluene-4-sulfonamide

Ni(C₆H₄ONCHC₆H₄N(CH₃)2)2

Pd(C₆H₄ONCHC₆H₄N(CH₃)2)2

Ru((C₅H₄N)2)2(OC₆H₄NCHC₆H₄N(CH₃)2)⁽¹⁺⁾*ClO₄^(1-)=[Ru((C₅H₄N)2)2(OC₆H₄NCHC₆H₄N(CH₃)2)]ClO₄

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