Technology Process of Methanone, bis[3-(dimethylamino)phenyl]-
There total 4 articles about Methanone, bis[3-(dimethylamino)phenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tin dichloride; hydrochloric acid; glacial acetic acid
2: NaOH-solution / man fuehrt das erhaltene methylschwefelsaure Salz mit Kaliumjodid in das entsprechende Jodid ueber und erhitzt letzteres im Vakuum
With
hydrogenchloride; sodium hydroxide; acetic acid; tin(ll) chloride;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: concentrated sulfuric acid / 130 - 140 °C / Reinigung durch Behandeln mit Aceton
2: glacial acetic acid; water; chromic acid
3: tin dichloride; hydrochloric acid; glacial acetic acid
4: NaOH-solution / man fuehrt das erhaltene methylschwefelsaure Salz mit Kaliumjodid in das entsprechende Jodid ueber und erhitzt letzteres im Vakuum
With
hydrogenchloride; sodium hydroxide; sulfuric acid; water; chromic acid; acetic acid; tin(ll) chloride;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: concentrated sulfuric acid / 130 - 140 °C / Reinigung durch Behandeln mit Aceton
2: glacial acetic acid; water; chromic acid
3: tin dichloride; hydrochloric acid; glacial acetic acid
4: NaOH-solution / man fuehrt das erhaltene methylschwefelsaure Salz mit Kaliumjodid in das entsprechende Jodid ueber und erhitzt letzteres im Vakuum
With
hydrogenchloride; sodium hydroxide; sulfuric acid; water; chromic acid; acetic acid; tin(ll) chloride;