N,N'-Bis(5-amino-2-methylphenyl)urea

Base Information

Chemical Name:N,N'-Bis(5-amino-2-methylphenyl)urea
CAS No.:96616-17-0
Molecular Formula:C15H18N4O
Molecular Weight:270.334
Hs Code.:
DSSTox Substance ID:DTXSID60544273
Nikkaji Number:J802.431F
Wikidata:Q82421347

Synonyms:N,N'-Bis(5-amino-2-methylphenyl)urea;96616-17-0;SCHEMBL11321386;DTXSID60544273;AKOS024286339

Suppliers and Price of N,N'-Bis(5-amino-2-methylphenyl)urea

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N,N'-Bis(5-amino-2-methylphenyl)urea

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:270.14806121
Heavy Atom Count:20
Complexity:306

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)N)NC(=O)NC2=C(C=CC(=C2)N)C

Technology Process of N,N'-Bis(5-amino-2-methylphenyl)urea

There total 2 articles about N,N'-Bis(5-amino-2-methylphenyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 96616-16-9
N,N'-bis(2-methyl-5-nitrophenyl)urea

: 96616-17-0
N,N'-bis(5-amino-2-methylphenyl)urea

Guidance literature:: With hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide; at 25 ℃; under 2280 Torr;
DOI:10.1021/jm00149a032

Reference yield:

: 99-55-8
2-methyl-5-nitroaniline

: 96616-17-0
N,N'-bis(5-amino-2-methylphenyl)urea

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / triethylamine / dioxane; benzene / 12 h / Heating

2: 71 percent / H₂ / 10percent Pd/C / dimethylformamide / 25 °C / 2280 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00149a032